Agaro-oligosaccharide iron and preparation method thereof

An agar oligosaccharide and agar technology, which can be used in the fields of antitoxins, metabolic diseases, drug combinations, etc., can solve the problems of single product function and low bioavailability, and achieve the purpose of activating cells, improving chelation rate, and promoting absorption. Effect

Active Publication Date: 2019-02-01
FUJIAN AGRI & FORESTRY UNIV
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  • Abstract
  • Description
  • Claims
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AI Technical Summary

Problems solved by technology

[0005] The purpose of the present invention is to provide a kind of iron agarose oligosaccharide and its preparation method for the outstanding problems...

Method used

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  • Agaro-oligosaccharide iron and preparation method thereof
  • Agaro-oligosaccharide iron and preparation method thereof

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preparation example Construction

[0019] A kind of preparation method of agar oligosaccharide iron, concrete steps are:

[0020] (1) Refining of Gracilaria agar: Use ultra-pure water to prepare gracilola agar into a 3~5wt% glue solution, heat to 90°C and stir until completely dissolved, add to the glue solution with a mass ratio of 10%~20% Polyethylene glycol 6000 and 1% NaCl clarifying agent were treated with ultrasonic vibrator at 20kHz~40kHz for 3min~8min, cooled to room temperature, centrifuged after static precipitation, and the separated liquid was treated with the same clarification, ultrasonic vibration and then static Centrifuge after placing the precipitate, combine the precipitate, wash the precipitate twice with cold water, press filter and dehydrate to obtain refined agar;

[0021] (2) Acid degradation: use ultrapure water to prepare refined agar gel into 3~5wt% glue solution, heat to 90°C and stir until completely dissolved, add HCl solution with a final concentration of 1.0 mol / L, treat for 90 m...

Embodiment 1

[0027] (1) Refining of Gracilaria agar: Use ultra-pure water to prepare a 5wt% glue solution of Gracilaria agar, heat it to 90°C and stir until completely dissolved, add polyethylene glycol with a mass ratio of 20% to the glue solution 6000 and 1% NaCl clarifying agent, use ultrasonic vibrator to process at 40kHz for 3min, cool to room temperature, centrifuge after standing and settling, take the separated liquid and use the same clarification, ultrasonic vibration treatment, settling and settling, then centrifuge, combine the precipitate, Wash the precipitate twice with cold water, press filter and dehydrate to obtain refined agar;

[0028] (2) Acid degradation: use ultrapure water to prepare refined agar gel into a 5wt% glue solution, heat to 90°C and stir until completely dissolved, add HCl solution with a final concentration of 1.0 mol / L, treat for 90 minutes, add dropwise 1.0mol / L L NaOH solution to a pH of 7, centrifuged at 7000 r / min for 15 min, and took the supernatant...

Embodiment 2

[0034] (1) Refining of Gracilaria agar: Use ultra-pure water to prepare Gracilaria agar into a 4wt% glue solution, heat to 90°C and stir until completely dissolved, add polyethylene glycol with a mass ratio of 15% to the glue solution 6000 and 1% NaCl clarifier, use an ultrasonic vibrator to process at 30kHz for 5min, cool to room temperature, let it stand for precipitation and then centrifuge, take the separated liquid and perform the same clarification, ultrasonic vibration treatment and then stand for precipitation and then centrifuge, combine the precipitate, Wash the precipitate twice with cold water, press filter and dehydrate to obtain refined agar;

[0035](2) Acid degradation: use ultrapure water to prepare refined agar gel into 4wt% glue solution, heat to 90°C and stir until completely dissolved, add HCl solution with a final concentration of 1.0 mol / L, treat for 90 minutes, add dropwise 1.0 mol / L L NaOH solution to a pH of 7, centrifuged at 7000 r / min for 15 min, an...

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Abstract

The invention discloses agaro-oligosaccharide iron and a preparation method thereof. The agaro-oligosaccharide iron is prepared by using Gracilaria agar as a raw material through steps of refining, acid degradation, high-pressure pulse electric field-assisted chelation, membrane separation, freeze-drying and pulverization. The refining step increases the neutral sugar content significantly, and after acid degradation, the chelation of agaro-oligosaccharide and iron ions can be promoted under the catalysis of a high-voltage pulsed electric field. The method has advanced and reasonable technology and high production efficiency; the prepared agaro-oligosaccharide iron product has high iron content, has good oxidation resistance to enhance cell viability, and promotes the iron absorption by body, and has high bioavailability.

Description

technical field [0001] The invention relates to the field of food processing, in particular to a preparation method of agar oligosaccharide iron. Background technique [0002] Iron is one of the essential trace elements for the human body. It is an essential component of hemoglobin and plays an important role in the transport of oxygen in the human body, the synthesis of deoxyribonucleic acid, and energy metabolism. Iron deficiency can lead to iron deficiency anemia or dysfunction. Studies have shown that 30% of the world's population suffers from iron deficiency, 46% of children aged 5-14 and 48% of pregnant women suffer from iron deficiency anemia. At present, the prevention and treatment of iron deficiency anemia is mainly achieved through the intake of iron supplements. Common iron supplements include ferrous sulfate, ferrous chloride, ferrous gluconate, etc. Although these iron supplements have high iron content, their stability is poor, and they are prone to produce ...

Claims

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Application Information

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IPC IPC(8): C08B37/12A61P39/06A61P3/02
CPCA61P3/02A61P39/06C08B37/0039
Inventor 宋洪波何洪安凤平黄群贾时荣孔钰婷
Owner FUJIAN AGRI & FORESTRY UNIV
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