High-density fireproof silicone adhesive and preparation process thereof
A silicone rubber, high-density technology, applied in the rubber field, can solve problems such as inconvenience, high price, and unenvironmental protection, and achieve the effects of broad application prospects, low production cost, and good radiation resistance.
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Embodiment 1
[0020] A one-component condensation type silicone rubber with high density and fire resistance, including the following raw materials in parts by weight: 100 parts of 107 rubber, 5 parts of 201 silicone oil, 150 parts of micaceous iron oxide, 80 parts of quartz powder, and 5 parts of fumed white carbon black , 10 parts of crosslinking agent, 1.5 parts of aminopropyltriethoxysilane and 0.1 part of catalyst. The crosslinking agent includes methyl tributylketoxime silane and vinyl tributylketoxime silane, and the mass ratio of methyl tributylketoxime silane to vinyl tributylketoxime silane is 4:1.
[0021] The viscosity of 107 glue is 8000CS, the weight fraction of hydroxyl group is 0.06%, the viscosity of 201 silicone oil is 500CS, the particle size of mica iron oxide is 10 mesh-1000 mesh, the particle size of quartz powder is 10-10000 mesh, fumed The specific surface area is 150 square meters per gram.
[0022] Disperse 107 glue, 201 silicone oil, micaceous iron oxide and quar...
Embodiment 2
[0024] A one-component condensation type silicone rubber with high density and fire resistance, including the following raw materials in parts by weight: 100 parts of 107 glue, 10 parts of 201 silicone oil, 120 parts of mica iron oxide, 50 parts of quartz powder, 100 parts of nano calcium carbonate, 8 parts of methyltrimethylsilane, 1.5 parts of glycidylmioxypropyltrimethoxysilane and 0.4 parts of catalyst.
[0025] The viscosity of 107 glue is 8000CS, the weight fraction of hydroxyl group is 0.06%, the viscosity of 201 silicone oil is 500CS, the particle size of mica iron oxide is 10 mesh-1000 mesh, the particle size of quartz powder is 10-10000 mesh, and the The particle size is 40-60 microns.
[0026] Disperse 107 glue, 201 silicone oil, micaceous iron oxide, nano-calcium carbonate and quartz powder in a mixer, and then lower the temperature at 150 degrees Celsius for 3 hours at a vacuum of minus 0.05 MPa to obtain the first mixture. After the mixture is cooled to room tem...
Embodiment 3
[0028] A two-component condensation type silicone rubber with high density and fire resistance, including the following raw materials in parts by weight: 100 parts of 107 rubber, 5 parts of 201 silicone oil, 100 parts of mica iron oxide, 80 parts of quartz powder, and 0.5 parts of fumed white carbon black , 30 parts of tetraethoxysilane, 20 parts of coupling agent and 0.1 part of catalyst. The coupling agent comprises glycidylmioxypropyltrimethoxysilane and aminopropyltriethoxysilane, and the mass ratio of glycidylmioxypropyltrimethoxysilane and aminopropyltriethoxysilane is 1:1.
[0029] The viscosity of 107 glue is 750CS, the weight fraction of hydroxyl group is 0.2%, the viscosity of 201 silicone oil is 350CS, the particle size of micaceous iron oxide is 10-1000 mesh, and the particle size of quartz powder is 10-10000 mesh.
[0030] Disperse 107 glue, 201 silicone oil, micaceous iron oxide, fumed silica and quartz powder evenly in a mixer, then lower the vacuum degree to n...
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