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A functional fiber and its microfluidic spinning device and fiber preparation method

A spinning device and microfluidic control technology, applied in fiber processing, stretch spinning, fiber chemical characteristics, etc., can solve the problems of long time consumption in the transfer process, limited application range, difficult to realize fiber design, etc., and achieve the preparation method Simple and novel, good repeatability and controllable structure

Active Publication Date: 2021-12-31
QINGDAO UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The phase separation method is to obtain a nanoporous foam through several steps such as dissolution, gelation, extraction, coagulation and drying, and the solid polymer is transferred into the foam pores to obtain polymer nanofibers; like the self-assembly method, its The disadvantage is that the transfer process takes too long
Mechanical stretching can produce very long single fiber filaments, but only those viscoelastic materials that can withstand large enough stress stretching deformation may use this method, which limits the range of applications
The operation method of electrospinning method is relatively simple, and it can continuously spin fiber filaments, but it has high requirements for equipment and production environment, and poor controllability. fiber for design

Method used

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  • A functional fiber and its microfluidic spinning device and fiber preparation method
  • A functional fiber and its microfluidic spinning device and fiber preparation method
  • A functional fiber and its microfluidic spinning device and fiber preparation method

Examples

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Effect test

preparation example Construction

[0040] A microfluidic spinning preparation method of a structure controllable function designable fiber of the present invention comprises the following steps:

[0041] (1) The spinning solution or coagulation solution with a mass fraction of 0.1-30% is poured into the spinning tank sequentially, and left to stand for degassing for 0.5-3 hours to obtain the spinning solution or coagulation solution for microfluidic spinning;

[0042] (2) The computer 1 controls the propeller of the spinning pot through the solenoid valve 2, and the speed of the propeller is 0.05-100mm / min, so as to realize the design of the fiber components online;

[0043] (3) The spinning solution or coagulation solution enters the microfluidic spinning chip through the spinning solution pipeline at a flow rate of 0.1-100mL / min, and converges in the common spinning solution pipeline 14 to form nascent fibers;

[0044] (4) The as-spun fibers are drawn through the airflow gathering drafting zone 13, and after ...

Embodiment 1

[0051] See attached figure 1 , a microfluidic spinning preparation method of a structure controllable function designable fiber of the present invention, comprising the following steps:

[0052] 1) According to the structure of the designed functional fiber, the microfluidic chip 12 is taken, and the microfluidic chip 12 has six spinning solution pipelines, which are respectively the first spinning solution pipeline 5, the second spinning solution pipeline 6, and the third spinning solution pipeline. The spinning solution pipeline 7, the fourth spinning solution pipeline 8, the fifth spinning solution pipeline 9, and the sixth spinning solution pipeline 10, these six spinning solution pipelines are all connected with the common spinning solution pipeline 14;

[0053] The six spinning liquid pipelines of the microfluidic chip 12 are all provided with corresponding spinning pots and propellers connected with the spinning pots, which are respectively the first propeller and the s...

Embodiment 2

[0065] On the basis of Example 1, the components of the spinning solution, the mass concentration, the speed of the propeller, the flow rate of the spinning solution and the flow through the pipeline were adjusted.

[0066] In this embodiment, the spinning solution includes spinning solution A and spinning solution B, and the spinning solution A is a chitosan solution with a mass concentration of 2%, and its preparation method is: take chitosan, dissolve in 5% In the acetic acid aqueous solution, stand defoaming to obtain chitosan solution; the spinning solution B is a graphene solution with a mass fraction of 0.1%, and its preparation method is: take a certain amount of self-made graphene and dissolve it in water, and ultrasonically disperse it for 10 minutes to obtain graphene solution.

[0067] In the present embodiment, in the present embodiment, the spinning solution A is packed into the second propeller and the spinning tank in the spinning tank 16 and the third propelle...

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Abstract

The invention discloses a functional fiber, a microfluidic spinning device and a fiber preparation method thereof. The microfluidic spinning device of the present invention includes a control mechanism, a nascent fiber forming mechanism, an airflow gathering and drafting mechanism, and a finishing and winding mechanism; the fiber preparation method includes sequentially injecting spinning liquid or coagulation liquid into a spinning tank, standing still Degassing; the fiber component design is realized online through the control mechanism; the spinning solution or coagulation solution enters the microfluidic spinning chip through the spinning solution pipeline, and gathers in the common spinning solution pipeline to form primary fibers; the primary fibers are sequentially passed through the airflow Concentrated drafting area drafting, curing, fiber heating dryer drying, and finally winding to the winding roller, so that the structure controllable function can design the fiber. The microfluidic spinning device of the present invention designs the fiber structure through programming, the preparation method is controllable, and realizes the complex structure and multifunctionality that are difficult to realize by other spinning methods. The preparation process is simple, the repeatability is good, and the application field is wide.

Description

technical field [0001] The present invention relates to the technical field of microfluidic spinning, in particular to a microfluidic spinning device for fibers with controllable structure and designable functions, a method for preparing fibers spun on the device and the obtained structure controllable functions Designable fibers. Background technique [0002] The structure of the fiber determines some properties of the fiber to a certain extent. For example, the cross section of the cotton fiber is round and hollow inside. This structure makes the cotton fiber have good warmth retention, air permeability, hygroscopicity and dyeing performance; the cross section of the silk is Composed of two silk fibroin coated with sericin, the special structure formed by the triangular cross-section of silk fibroin and the lamellar structure of sericin makes silk have a luster that cannot be compared with other fibers. In order to obtain the good properties of this kind of natural fibers...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D01D1/09D01D5/14D01D5/253D01D5/30D01D5/34D01D5/32D01F8/18D01F8/16D01F8/12
CPCD01D1/09D01D5/14D01D5/253D01D5/30D01D5/32D01D5/34D01F8/12D01F8/16D01F8/18
Inventor 田明伟胡希丽曲丽君朱士凤张宪胜刘士广孙亚宁
Owner QINGDAO UNIV
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