Brake disc prepared from QICC nano carbon-carbon SiC nano redundant composite material and preparation method
A technology of composite materials and brake discs, which is applied in the direction of mechanical equipment, friction linings, gear transmission mechanisms, etc., can solve the problems of long cycle time, high unit cost, and cumbersome process
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Embodiment 1
[0029] Under vacuum conditions, put the carbon fiber in an environment of 2150 ° C for 2 h, soak the calcined carbon fiber matrix with a mixed solution of sodium hydroxide and sodium sulfite at 50 ° C for 60 min, then rinse it with deionized water until it is neutral, and dry it until use.
[0030] Take 10ml of the composite catalyst, add 90ml of ammonia water with a concentration of 2mol / L, and then add 30ml of absolute ethanol, stir to make it evenly mixed.
[0031] The mixed solution was transferred to an autoclave, the obtained C / C-SiC carbon fiber prefabricated body was immersed in the autoclave for 8 hours, and the autoclave was immersed in oil at 120° C. for 2 hours. Rapidly cool the reactor with cold water to lower the temperature to normal / room temperature, take out the carbon fiber prefabricated body and dry it naturally in the shade while continuously turning it. The obtained sample is transferred to a vacuum carbon tube furnace for calcination, and reduced to obta...
Embodiment 2
[0041] Under vacuum conditions, place the carbon fiber in an environment of 2300°C for 3h and calcine the calcined carbon fiber matrix with a mixed solution of sodium hydroxide and sodium sulfite at 70°C for 80min, then wash it with deionized water until neutral, and finally dry it stand-by.
[0042] Take 13ml of composite catalyst, add 120ml of ammonia water with a concentration of 2mol / L, then add 50ml of absolute ethanol, stir to make it evenly mixed.
[0043] The mixed solution was transferred to an autoclave, and the obtained C / C-SiC carbon fiber preform was immersed in the autoclave for 10 hours, and the autoclave was immersed in oil at 150° C. for 3 hours. Rapidly cool the reactor with cold water to lower the temperature to normal / room temperature, take out the carbon fiber prefabricated body and dry it naturally in the shade while continuously turning it. The obtained sample is transferred to a vacuum carbon tube furnace for calcination, and reduced to obtain a nano-c...
Embodiment 3
[0053] Under vacuum conditions, put the carbon fiber into an environment of 2200 ° C for 2 h, soak the calcined carbon fiber matrix with a mixed solution of sodium hydroxide and sodium sulfite at 60 ° C for 70 min, then rinse it with deionized water until it is neutral, and finally dry it stand-by.
[0054] Take 13ml of composite catalyst, add 100ml of ammonia water with a concentration of 2mol / L, then add 40ml of absolute ethanol, stir to make it evenly mixed.
[0055] The mixed solution was transferred to an autoclave, the obtained C / C-SiC carbon fiber preform was immersed in the autoclave for 8 hours, and the autoclave was immersed in oil at 130° C. for 2 hours. Rapidly cool the reactor with cold water to lower the temperature to normal / room temperature, take out the carbon fiber prefabricated body and dry it naturally in the shade while continuously turning it. The obtained sample is transferred to a vacuum carbon tube furnace for calcination, and reduced to obtain a nano...
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