A kind of wear-resistant milk protein fiber and its fabric preparation method and application
A milk protein fiber and casein technology, applied in the field of textiles, can solve the problems of local skin wrinkles, difficult to penetrate the adhesive tape, poor air permeability of the adhesive tape, etc. Effect
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment 1
[0037] A preparation method of wear-resistant milk protein fiber, comprising the steps of:
[0038] a. Add 20kg of polyacrylonitrile fibers into ammonia water and stir for 16min at a stirring temperature of 80°C, filter, wash until neutral, and dry, then add 2kg of bromoacetyl bromide, 3kg of phosphorus oxychloride, and 5kg of phenylphosphonic dichloride, Raise the temperature to 120°C, keep it warm for 30 minutes, wash until neutral, and dry to obtain acid halide polyacrylonitrile;
[0039] b. Add 2kg of casein and 0.2kg of acid halide polyacrylonitrile into 4kg of water, grind for 14min, the grinding temperature is 50°C, the grinding pressure is 0.16MPa, add water until the water content is 65wt%; adjust the pH to 8.5-9.5 under nitrogen protection , stirred for 8 minutes, and the stirring temperature was 80°C; then, 0.18kg of ethylene glycol diglycidyl ether was added under oxygenated state, ultrasonically treated for 4 minutes, then adjusted to 120°C and stirred for 10 minu...
Embodiment 2
[0041] A preparation method of wear-resistant milk protein fiber, comprising the steps of:
[0042] a. Add 30kg of polyacrylonitrile fibers to 4mol / L sodium carbonate aqueous solution and stir for 10min at a stirring temperature of 90°C, filter, wash until neutral, dry, then add 2kg of propionyl bromide, heat up to 128°C, and keep warm for 20min , washed to neutrality, and dried to obtain acid halide polyacrylonitrile;
[0043]b. Add 10kg of casein and 0.1kg of acid halide polyacrylonitrile into 10kg of water, grind for 10min, the grinding temperature is 60°C, the grinding pressure is 0.12MPa, add water until the water content is 75wt%; adjust the pH to 8.5-9.5 under nitrogen protection , stirred for 4 minutes, and the stirring temperature was 90°C; then 0.1kg of ethylene glycol diglycidyl ether was added under oxygenated state, ultrasonically treated for 12 minutes, then adjusted to 110°C and stirred for 18 minutes, filtered, washed, and dried at 40°C to constant weight, Wea...
Embodiment 3
[0045] A preparation method of wear-resistant milk protein fiber, comprising the steps of:
[0046] a. Add 21kg of polyacrylonitrile fibers into triethylamine and stir for 15min at a stirring temperature of 81°C, filter, wash until neutral, and dry, then add 2kg of thionyl chloride, 3kg of oxalyl chloride, 1kg of chloroacetyl chloride, 3kg of 2- Bromoisobutyryl bromide, heat up to 121°C, keep warm for 29 minutes, wash until neutral, and dry to obtain acid halide polyacrylonitrile;
[0047] b. Add 3kg of casein and 0.19kg of acid halide polyacrylonitrile into 5kg of water, grind for 13.5min, the grinding temperature is 51°C, the grinding pressure is 0.155MPa, add water until the water content is 66wt%; adjust the pH to 8.5- 9.5, stirring for 7 minutes, the stirring temperature is 81°C; then add 0.17kg of ethylene glycol diglycidyl ether under oxygenated state, ultrasonic treatment for 5 minutes, then adjust the temperature to 119°C and stir for 12 minutes, filter, wash, and dry...
PUM
Property | Measurement | Unit |
---|---|---|
area | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com