Synthesis method and application method of manganese Prussian blue analog material for lithium ion battery
A technology similar to Prussian blue and lithium-ion batteries, which is applied in the synthesis and application of manganese-based Prussian blue materials for lithium-ion batteries. It can solve the problems of limited theoretical capacity and poor cycle stability of graphite materials, and achieve improved electrochemical performance. Reduced reaction time and reduced production costs
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Embodiment 1
[0053] Example 1: Preparation method and structural characterization of manganese-based Prussian blue-like materials for lithium-ion batteries
[0054] The source of manganese is anhydrous manganese chloride (MnCl 2 ), ferricyanide comes from potassium ferricyanide (K 3 [Fe(CN) 6 ]), the chelate selects sodium citrate dihydrate;
[0055] Weigh three 1mmol anhydrous manganese chloride (MnCl 2 ) and 2mmol sodium citrate dihydrate were completely dissolved in 25ml, 50ml, and 100ml deionized water respectively to obtain colorless, clear and transparent solution A, solution B and solution C respectively. Another weighed 1mmol potassium ferricyanide (K 3 [Fe(CN) 6 ]) was dissolved in 25ml of deionized water to obtain solution D. After stirring and dissolving completely, pour C part of solution D into solution A, solution B and solution C respectively to obtain solution E, solution F and solution G respectively, and stand still at room temperature After 12 hours, they were coll...
Embodiment 2
[0062] Embodiment 2: weigh 1mmol anhydrous manganese chloride (MnCl 2 ), 2mmol sodium citrate dihydrate was completely dissolved in 25ml deionized water to obtain a colorless, clear and transparent solution A. Weigh again 1mmol potassium ferricyanide (K 3 [Fe(CN) 6 ]) was dissolved in 25ml of deionized water to obtain solution B, and solution B was poured into solution A and mixed evenly to obtain solution C, which was left to stand at room temperature for 6 hours, separated and purified, and dried at 60°C for 12 to 24 hours to obtain white powder product. The product is manganese-like Prussian blue, the microscopic shape is cubic, and the microscopic particle size is 150-180nm.
Embodiment 3
[0063] Embodiment 3: weigh 0.5mmol manganese chloride monohydrate (MnCl 2 ·H 2 (0), 2mmol anhydrous sodium citrate was completely dissolved in 25ml deionized water to obtain a colorless, clear and transparent solution A. Weigh again 1mmol potassium ferricyanide (K 3 [Fe(CN) 6 ]) was dissolved in 25ml deionized water to obtain solution B, and solution B was poured into solution A and mixed uniformly to obtain solution C, which was left to stand at room temperature for 24 hours to obtain the final white powder product. The product is a manganese-like Prussian blue with a cubic microscopic shape and a particle size distribution of 310-410nm.
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