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56 results about "Sodium citrate dihydrate" patented technology

Sigma-Aldrich offers a number of Sodium citrate dihydrate products. View information & documentation regarding Sodium citrate dihydrate, including CAS, MSDS & more.

Method for preparing carbon-material-carrying tin dioxide nanosheet composite material

The invention relates to a method for preparing a carbon-material-carrying tin dioxide nanosheet composite material, belonging to the technical field of functional composite materials. According to the method, a carbon material, tin dichloride dihydrate and sodium citrate dihydrate are taken as raw materials and are subjected to mixing, stirring, hydrothermal synthesis, solid-liquid separation, cleaning and drying, and then, the morphology-controlled carbon-material-carrying tin dioxide nanosheet composite material is prepared. The method provided by the invention is simple and is convenient in operation; and water is taken as a solvent, so that the production cost is lower, the environment is not polluted, and the popularization and the application are facilitated. The carbon-material-carrying tin dioxide nanosheet composite material prepared by adopting the method provided by the invention can be widely applied to new-energy devices such as lithium ion batteries, solar batteries and supercapacitors, and can also be applicable to the fields of catalyst carriers, information materials and the like.
Owner:CHONGQING UNIV

Synthesis method and application method of manganese Prussian blue analog material for lithium ion battery

The invention discloses a synthesis method and application method of manganese Prussian blue material for a lithium ion battery, and belongs to the preparation and application method of the manganesePrussian blue material. The synthesis method comprises the following steps: selecting a manganese source from anhydrous manganese chloride (MnCl2) or manganese chloride monohydrate (MnCl2.H2O); selecting an iron source and cyanogen from potassium ferricyanide (K3[Fe(CN)6]); selecting a chelating agent from anhydrous sodium citrate or sodium citrate dihydrate; weighing the manganese source and theclelating agent in mass ratio of x: 1, and dissolving into a mixed solution with the methyl alcohol and deionized water in any proportion to prepare a solution A; dissolving the potassium ferricyanideinto the deionized water to prepare the solution B with the concentration of 0.04mol / L; pouring the solution B into the solution A, uniformly mixing to acquire the solution C, standing for 6-24h at the room temperature, and separating, purifying and drying to obtain a target product. The synthesis method disclosed by the invention has the advantages that the raw material is easy to obtain, the synthesis method is simple, the operation step is high in controllability, the obtained product is high in purity, and uniform in particle size; and the structure is a hollow cube and easy to prepare ina large-scale manner. The manganese Prussian blue material disclosed by the invention is served as the lithium ion battery negative material, and is excellent in electrochemical performance.
Owner:CHINA UNIV OF MINING & TECH

Method for reducing metal ion with nanosilicate platelets and dispersing metal nanoparticle and product thereof

The present invention provides a method for reducing metal ions (for example, silver ions) and stably dispersing metal nanoparticles by nanosilicate platelets. An organic dispersant, nanosilicate platelets and a metal ionic solution are mixed to perform a reductive reaction, wherein the organic dispersant is tri-sodium citrate dihydrate (SCD), chitosan or polyvinyl pyrrolidone (PVP), to produce a mixture of stably dispersed metal nanoparticles.
Owner:NAT TAIWAN UNIV

High strength, density controlled cold fusion concrete cementitious spray applied fireproofing

ActiveUS9670096B1Reduce quality lossDecreasing mixture cohesive (wet) shear strength rheologyFireproof paintsSolid waste managementSlagMetasilicate
A density controlled cold fusion concrete cementitious spray applied fireproofing material including a mixture of water, one or more of silicon dioxide, expanded glass, vermiculite, bottom ash, perlite, expanded shale, or other lightweight aggregates of various diameter sizes ranging from about 0.025 mm to about 12.5 mm in diameter; anhydrous or hydrous sodium or potassium metasilicate; waste from steel production consisting of Granulated Ground Blast Furnace Slag (GGBFS); high calcium or low calcium waste from coal combustion (fly ash or bottom ash); sodium tetraborate, sodium citrate dihydrate, citric acid, or boric acid; and an alkali-resistant micro-.
Owner:GEOPOLYMER SOLUTIONS LLC

Fire resistant coating

A density controlled cold fusion concrete cementitious spray applied fireproofing material including a mixture of water, one or more of silicon dioxide, expanded glass, vermiculite, bottom ash, perlite, expanded shale, expanded polystyrene, and sulfonated formaldehyde, or other lightweight aggregates of various diameter sizes ranging from about 0.025 mm to about 12.5 mm in diameter; anhydrous or hydrous sodium or potassium metasilicate; waste from steel production consisting of Granulated Ground Blast Furnace Slag (GGBFS); high calcium or low calcium waste from coal combustion (fly ash or bottom ash); sodium tetraborate, sodium citrate dihydrate, citric acid, or boric acid; and an alkali-resistant micro-fiber.
Owner:GEOPOLYMER SOLUTIONS LLC

Micro-nano structure zinc oxide-carbon composite pellet and preparation method thereof

The invention discloses a micro-nano structure zinc oxide-carbon composite pellet and a preparation method thereof. The micro-nano structure zinc oxide-carbon composite pellet is obtained by hybridization compounding of zinc oxide and carbon to obtain a solid pellet having the diameter of 6-12 micrometers, wherein vertical nanosheets having the length of 700-900 nanometers, the height of 700-900 nanometers and the thickness of 15 to 25 nanometers are formed on surfaces of the solid pellet and are connected with each other into a nest; a mole ratio of zinc oxide to carbon is (60-70%): (30-40%); zinc oxide has a hexagonal structure; and carbon comprises amorphous carbon and graphitized carbon and a weight ratio of the amorphous carbon to the graphitized carbon is (85-95%): (5-15%). The preparation method comprises the following steps of dissolving zinc acetate dihydrate, urea, sodium citrate dihydrate and glucose in water to obtain a mixed solution, carrying out hydrothermal treatment on the mixed solution to obtain a reaction solution, orderly carrying out solid-liquid separation, washing and drying to obtain an intermediate product, putting the intermediate product in an inert gas atmosphere, and carrying out annealing to obtain the micro-nano structure zinc oxide-carbon composite pellet. The micro-nano structure zinc oxide-carbon composite pellet can be widely used for fields of catalysis, adsorption and photoelectricity.
Owner:HEFEI INSTITUTES OF PHYSICAL SCIENCE - CHINESE ACAD OF SCI +1

High strength, density controlled cold fusion concrete cementitious spray applied fireproofing

A density controlled cold fusion concrete cementitious spray applied fireproofing material including a mixture of water, one or more of silicon dioxide, expanded glass, vermiculite, bottom ash, perlite, expanded shale, or other lightweight aggregates of various diameter sizes ranging from about 0.025 mm to about 12.5 mm in diameter; anhydrous or hydrous sodium or potassium metasilicate; waste from steel production consisting of Granulated Ground Blast Furnace Slag (GGBFS); high calcium or low calcium waste from coal combustion (fly ash or bottom ash); sodium tetraborate, sodium citrate dihydrate, citric acid, or boric acid; and an alkali-resistant micro-.
Owner:GEOPOLYMER SOLUTIONS LLC

Cold fusion concrete

A cold fusion concrete formulation including a mixture of water, silicon based mineral aggregates acting as a filler material; sodium or potassium metasilicate / pentahydrate acting as an activator; waste from steel production including Granulated Ground Blast Slag acting as a cementitious ingredient; high calcium or low calcium waste from coal combustion (fly ash or bottom ash) acting as a cementitious ingredient; sodium tetraborate, sodium citrate dihydrate, citric acid, or boric acid acting as set-time retarders; strengthening agents including including calcium, potassium, magnesium, sodium, or aluminium hydroxides; attapulgite, kaolin, red, or other fine grained, high alumino silicate containing clay, for increasing the silicon and alumino-silicate concentration and associated strength; a protein or synthetic protein material to form a weak covalent bond with the hydroxides and silicates, for the purpose of maintaining a consistent volume during the curing process; and a pollinated fern oil to reduce water content of the mixture and decrease viscosity.
Owner:GEOPOLYMER SOLUTIONS LLC

Animal semen preservative with biological activity and preparation method thereof

The invention aims to provide an animal semen preservative with biological activity and a preparation method of the animal semen preservative. The animal semen preservative with the biological activity contains oligoprocyanidine so that the animal semen preservative has an anti-oxidation effect, can prolong the preservation time of semen and keeps the activity of animal sperms. The animal semen preservative is prepared by mixing 1000mL of a common medium and 16mg of oligoprocyanidine; the common medium is prepared by mixing 6 parts of glucose, 0.37 part of EDTA (Ethylene Diamine Tetraacetic Acid), 0.375 part of sodium citrate dihydrate, 0-0.12 part of sodium bicarbonate, 0.1 part of neomycin and 100 parts of distilled water; the neomycin is independently added before the semen is diluted. The formula contains the oligoprocyanidine so that the animal semen preservative has the anti-oxidation effect and can prolong the preservation time of the semen; the degradation of a semen sample can be relieved by the oligoprocyanidine and the oligoprocyanidine has no negative effects on the activity of the sperms, so that the activity of the animal sperms is kept; particularly, the survival rate of the sperms preserved at a low temperature is obviously improved.
Owner:LINYI SIKE BIOTECH

Cold fusion concrete

A cold fusion concrete formulation including a mixture of water, silicon based mineral aggregates acting as a filler material; sodium or potassium metasilicate / pentahydrate acting as an activator; waste from steel production including Granulated Ground Blast Slag acting as a cementitious ingredient; high calcium or low calcium waste from coal combustion (fly ash or bottom ash) acting as a cementitious ingredient; sodium tetraborate, sodium citrate dihydrate, citric acid, or boric acid acting as set-time retarders; strengthening agents including calcium, potassium, magnesium, sodium, or aluminium hydroxides; attapulgite, kaolin, red, or other fine grained, high alumino silicate containing clay, for increasing the silicon and alumino-silicate concentration and associated strength; a protein or synthetic protein material to form a weak covalent bond with the hydroxides and silicates, for the purpose of maintaining a consistent volume during the curing process; and a pollinated fern oil to reduce water content of the mixture and decrease viscosity.
Owner:GEOPOLYMER SOLUTIONS LLC

Light reflecting particles

Visible light reflecting particles comprise one or more detergent ingredients and a light reflecting component, which results in the particle having a specular visible light reflection which is greater in intensity than the specular visible light reflection of the ingredients per se. Preferably, the reflection is greater than the reflection of sodium citrate dihydrate, as defined herein. The reflecting particle preferably comprises the light reflecting component evenly applied on its surface. The particles are particularly suitable for incorporation into laundry or dish washing compositions, fabric conditioning compositions or hard-surface cleaning compositions.
Owner:THE PROCTER & GAMBLE COMPANY

Stable fasudil hydrochloride injection and preparation method thereof

The invention belongs to the field of pharmaceutical preparation, and particularly relates to stable fasudil hydrochloride injection and a preparation method thereof. The fasudil hydrochloride injection comprises fasudil hydrochloride, stabilizers, anhydrous citric acid, sodium citrate dihydrate, sodium chloride and water for injection, wherein the stabilizers comprise N-carboxymethyl chitosan and reduced glutathione according to the mass ratio of 1:(0.05-0.35). The preparation method includes the steps: dissolving components in the formula by the water for injection after pyrogen removal; adjusting pH (potential of hydrogen); adding medicinal carbon for stirring adsorption to further remove pyrogen and perform discoloration; performing filtration and decarburization; performing filtration, sterilization, sub-package, potting and sterilization to obtain the fasudil hydrochloride injection. The fasudil hydrochloride injection has fine light stability and simple in formula, insoluble particles are effectively suppressed, the preparation process is easily operated, and industrialization is facilitated.
Owner:中润药业有限公司

Molybdenum disulfide and titanium dioxide-modified ferroferric oxide nanometer composite material

InactiveCN108003966AImprove the lubrication effectExcellent electrorheological propertiesAdditivesThioureaCitrinin hydrate
The invention belongs to the technical field of functional composite materials and relates to a preparation technology of a shear thinning rheological property material, in particular to a molybdenumdisulfide and titanium dioxide-modified ferroferric oxide nanometer composite material. The molybdenum disulfide and titanium dioxide-modified ferroferric oxide nanometer composite material comprisesthe following raw materials in part by weight: 3-8 parts of ferric chloride hexahydrate, 5-15 parts of anhydrous sodium acetate, 0.1-1 part of sodium citrate dihydrate, 0.1-0.5 part of ammonium molybdate tetrahydrate, 0.5-1.0 part of thiourea, 0.5-2.0 parts of tetrabutyl titanate and 100-150 parts of ethylene glycol; titanium dioxide and molybdenum disulfide have excellent electro-rheological properties and can generate higher shear yield stress under the action of an electric field; meanwhile, magnetic ferroferric oxide has higher magnetic saturation degree and can generate higher shear yieldstress under the action of a magnetic field; the molybdenum disulfide has excellent lubricating property; therefore, the molybdenum disulfide and titanium dioxide-modified ferroferric oxide nanometercomposite material is low in cost, clean, non-toxic and shorter in reaction time and has wide application value.
Owner:QINGDAO HAICHENG INTPROP SERVICES CO LTD

Biosynthesis method of cadmium selenide quantum dots

The invention discloses a biosynthesis method of cadmium selenide quantum dots. The biosynthesis method comprises the following steps: by adopting selenite as an Se source, water-soluble salts of cadmium as a Cd source, a mercapto compound as a stabilizer and wet thalli obtained by carrying out fermentation culture on escherichia coli and saccharomycete as a catalyst, under the action of sodium citrate dihydrate, culturing in an escherichia coli fermentation medium or a saccharomycete fermentation medium at 37 DEG C for 1-6 days, centrifuging, discarding the supernatant, and collecting the precipitate to obtain cadmium selenide quantum dots. By virtue of the biosynthesis method disclosed by the invention, cadmium selenide quantum dots, which have adjustable and uniform size, good biocompatibility and high luminescence, are synthesized, and cadmium selenide quantum dots can be applied to dying of saccharomycete, the quantum dots show size-dependent luminescent properties, the diameter of quantum dots is about 5nm, quantum dots show a good single crystal structure under a high-resolution transmission electron microscopy and the quantum yield reaches 35%.
Owner:HANGZHOU NORMAL UNIVERSITY

Poly-ionic-liquid-modified cerium-doped nano zinc oxide photocatalyst and preparation method and application thereof

The invention relates to a poly-ionic-liquid-modified cerium-doped nano zinc oxide photocatalyst and a preparation method and application thereof. The preparation method comprises the steps of adopting zinc nitrate hexahydrate, hexamethylamine, sodium citrate dihydrate and cerium nitrate hexahydrate as raw materials; adopting 1-butyl sulfonate-3-vinyl imidazole bisulfate as poly-ionic liquid, using the poly-ionic liquid for preparing a mixture water solution, stirring the mixture at a constant temperature for a reaction, and then making the mixture subjected to centrifugation, washing, drying,roasting and grinding to obtain poly-ionic-liquid-modified cerium-doped nano zinc oxide powder. The poly-ionic-liquid-modified cerium-doped nano zinc oxide powder has more excellent photocatalytic activity during degrading of an organic dye under illumination of visible light in comparison with pure zinc oxide, and has the advantages of small particle size, high dispersity and stability and the like. A preparation technology is simple, raw materials are easily obtained, the preparation process is clean and free of pollution, and a prepared product has a broad application prospect in the aspect of organic dye wastewater disposal.
Owner:TAIZHOU UNIV

Carnauba wax-containing valnemulin injection

The invention relates to a carnauba wax-containing valnemulin injection with latex-like appearance. Each liter of the injection comprises 150-180g of valnemulin hydrochloride, 2.5-11g of carnauba wax, and the balance of glyceryl triacetate / benzyl benzoate / 1,2-propylene glycol / ethanol with a volume ratio of 4.5:3:3.3:1. Each of the injection also comprises 100-150ml of glyceryl monooleate. In the preparation process of 1L of the injection, 13.0-31.2g of sodium citrate dihydrate (C6H5Na3O7.2H2O) or 19.0-31.9g of sodium carbonate decahydrate (Na2CO3.10H2O) is added. Added sodium citrate or sodium carbonate reacts with valnemulin hydrochloride. Each liter of the injection prepared in the invention includes 150-180g of valnemulin alkali and valnemulin acid salt (hydrochloride or citrate), 2.5-11g of carnauba wax, 100-150ml of glyceryl monooleate, and the balance of glyceryl triacetate / benzyl benzoate / 1,2-propylene glycol / ethanol with a volume ratio of 4.5:3:3.3:1.
Owner:北京中农华威科技集团有限公司

Preparation method of nitrogen-doped porous carbon material and application of nitrogen-doped porous carbon material in super capacitor

The invention relates to a preparation method of a nitrogen-doped porous carbon material and an application of the nitrogen-doped porous carbon material in a super capacitor. The preparation method ofthe nitrogen-doped porous carbon material comprises the following steps of: respectively dissolving sodium alginate, sodium citrate dihydrate and melamine in water according to a molar ratio, mixing,ball-milling, uniformly mixing and freeze-drying to obtain a material A; calcining the material A in an inert gas atmosphere, and washing with hydrochloric acid and deionized water to obtain a material B; mixing the material B with KOH and calcining in the inert gas atmosphere to obtain the nitrogen-doped porous carbon material; mixing the prepared nitrogen-doped porous carbon material with a binder and a conductive agent according to the mass ratio, coating the mixture on a current collector, and drying the mixture in vacuum to obtain an electrode sheet; then, the electrode sheet is used aspositive electrode and negative electrode at the same time, and assembling into a symmetrical soft package super capacitor. The preparation process is simple, the cost is low, and the prepared nitrogen-doped porous carbon material has higher specific surface area and uniform pore size distribution, and has higher mass specific capacitance and better cycle stability and multiplying power performance when being used as an electrode material of the super capacitor.
Owner:NANCHANG UNIV

Oral quetiapine sustained-release tablet

The technical problem solved by the invention is to provide an oral sustained-release tablet of quetiapine and its salts which can effectively and continuously release for more than 12 hours, is slow in medical effect release, can stably maintain the effective plasma concentration for 24 hours, is long in release period, less in toxic or side effect, and convenient for administration; the main components are quetiapine with active components, a skeletal material with sustained-release effect, and an excipient; the invention is characterized in that on a basis of the total weight of the tablet, the tablet comprises 5%-50% of quetiapine with active components, 5%-50% of skeletal material with sustained-release effect, and 20%-50% of excipients. Polyoxyethylene with one or several different models is selected as the skeletal material. The excipient comprises a proper amount of sodium citrate dihydrate compounds. Polyoxyethylene is selected which can prolong the sustained-release period; the release period is greatly increased; the medicinal effect is released stably and slowly; the plasma concentration is guaranteed; the disease condition is controlled stably; patients are provided with 24-hour effective treatment; and the invention is widely applicable to single-dosage quetiapine treatment.
Owner:TIANJIN DEXUAN MEDICAL TECH

Citric acid antigen repairing solution

The invention relates to the technical field of immunohistochemistry and discloses a citric acid antigen repairing solution. Each 1000mL of the citric acid antigen repairing solution contains 0.35g-0.40g of citric acid monohydrate, 2.40g-2.42g of sodium citrate dihydrate, 400-600 microliters of Tween 20, 50-500mL of triethanolamine or ethylene glycol or trihydric alcohol and the balance of single-stage distilled water. The citric acid antigen repairing solution has good infiltration and repairing effects and can be used for repairing tissue slices with relatively less use amount; and the repaired tissue slices are easy to stain and the staining effect is good. The repairing solution is not easy to volatilize and can be matched with a full-automatic immunohistochemical instrument for utilization.
Owner:ZHEJIANG CENTURY CONDOR MEDICAL SCI & TECHNOLOTY CORP

Metallization layer structure for flip chip package

The present invention discloses a metallization layer structure for flip chip package, which comprises an UBM layer formed on a metal pad, whereby a fine-quality tin-based solder ball can be formed on the metal pad. The UBM layer is a NiZnP layer formed via the reduction and oxidization of a solution containing nickel sulfate (Ni2SO4), zinc sulfate (ZnSO4), sodium dihydrogen phosphite (NaH2PO2), sodium citrate dihydrate (Na3C6H5O7-2H2O), and ammonium chloride (NH4Cl). The present invention replaces the conventional Au / Ni—P dual-layer structure. Therefore, the present invention can decrease the complexity of the process and reduce the cost. Further, the metallization layer structure of the present invention is tough, hard to peel off and highly corrosion-resistant.
Owner:NATIONAL TSING HUA UNIVERSITY

Fire resistant coating

A density controlled cold fusion concrete cementitious spray applied fireproofing material including a mixture of water, one or more of silicon dioxide, expanded glass, vermiculite, bottom ash, perlite, expanded shale, expanded polystyrene, and sulfonated formaldehyde, or other lightweight aggregates of various diameter sizes ranging from about 0.025 mm to about 12.5 mm in diameter; anhydrous or hydrous sodium or potassium metasilicate; waste from steel production consisting of Granulated Ground Blast Furnace Slag (GGBFS); high calcium or low calcium waste from coal combustion (fly ash or bottom ash); sodium tetraborate, sodium citrate dihydrate, citric acid, or boric acid; and an alkali-resistant micro-fiber.
Owner:GEOPOLYMER SOLUTIONS LLC

Diluent preparation capable of prolonging normal-temperature survival time of boar semen

The invention provides a diluent preparation capable of prolonging the normal-temperature survival time of boar semen. The diluent preparation is prepared by adding an antioxidant into a basic diluent and mixing the antioxidant with the basic diluent, wherein the mass-volume ratio g / L of the antioxidant to the basic diluent is (0.03-0.15): 1. Each liter of the basic diluent contains the following raw materials by mass: 15.0-50.0 g of glucose, 0.5-5.0 g of ethylenediamine tetraacetic acid, 0.2-0.5 g of tea polyphenol, 5.0-15.0 g of sodium citrate dihydrate, 0.05-5.0 g of sodium bicarbonate and 0.02-3.0 g of potassium chloride. The antioxidant is prepared from apigenin, phenethyl caffeate, cumaric acid and plumbago zeylanica extract in a mass ratio of (0.3-0.8): (2-5): (1.3-2): 1. The basic raw materials and the dosage proportion of the diluent preparation are optimized, the survival time of the boar semen is prolonged under the normal temperature condition, sperm indexes related to the fertilization capacity are maintained, and the diluent preparation has certain guiding significance for obtaining high-quality, high-yield and low-cost boar semen stored at the normal temperature.
Owner:FUJIAN AGRI & FORESTRY UNIV +1

Ursolic acid magnetic molecularly imprinted nano-microsphere and method for extracting ursolic acid from dogwood

ActiveCN111253613ANo damage to biological activityStrong specificityOther chemical processesSteroidsMicrosphereUrsolic acid
The invention belongs to the field of biological separation and natural product extraction, and particularly relates to ursolic acid magnetic molecularly imprinted nano-microspheres and a method for extracting ursolic acid from dogwood. The preparation method of the ursolic acid magnetic molecularly imprinted nano-microspheres comprises the following steps: (1) preparing carboxyl modified magneticnano-microspheres by taking 1.5-5 wt% of ferric chloride hexahydrate and 0.5-2 wt% of sodium citrate dihydrate as raw materials and ethylene glycol as a solvent and adopting a hydrothermal synthesismethod; and (2) preparing the ursolic acid magnetic molecularly imprinted nano-microspheres from raw materials including the magnetic nano-microspheres. The ursolic acid magnetic molecularly imprintednano-microspheres provided by the invention have large ursolic acid adsorption capacity, can realize rapid separation of a target object in complex components by controlling a magnetic field, can effectively avoid repeated centrifugation, filtration and other procedures, and can effectively solve the problem of high extraction difficulty of ursolic acid in dogwood.
Owner:NANYANG NORMAL UNIV

Preparation method of earthy yellow (BiO)2CO3 multistage structure microsphere

The invention discloses a preparation method of an earthy yellow (BiO)2CO3 multistage structure microsphere, which comprises the following steps: magnets are put into a dry reaction kettle, ultrapurewater, sodium citrate dihydrate and Bi(NO3)3.5H2O are mixed and stirred to obtain a mixed solution; the pH of the mixed solution is adjusted with ammonia to maintain the pH of the mixed solution at 7-8 and the mixture is continuously stirred; at that end of stirring, the reaction kettle is tightened, put into an oven, and the mixture is hydrothermally reacted for 24 hours at 180 DEG C; as that reaction kettle is cooled to room temperature, centrifugal washing is performed with distilled water and anhydrous ethanol in turn, and then drying is carried out in a vacuum dry oven at 65 DEG C; the obtained earthy yellow (BiO)2CO3 multistage structure microspheres are obtained. The invention can not only effectively absorb heavy metal ions in the water environment, but also photocatalytically degrade organic pollutants in the water body and realize various environmental purification functions of a material through the earthy yellow (BiO) 2CO3 multistage structure microspheres controllably synthesized by the hydrothermal method.
Owner:WENZHOU UNIVERSITY

Method for rapidly determining fluoride content in drinking water surrounding furniture plant

The invention discloses a method for rapidly determining the fluoride content in the drinking water surrounding a furniture plant. The method comprises the steps of weighing standard sodium fluoride, and shifting sodium fluoride into a volumetric flask after dissolving sodium fluoride with water; weighing sodium acetate and dissolving sodium acetate in water; weighing sodium citrate dihydrate and sodium nitrate, dissolving sodium citrate dihydrate and sodium nitrate in water, and adjusting the pH value with hydrochloric acid; siphoning off a proper amount of water sample by a pipette, placing the water sample in the volumetric flask, and adjusting the pH value to be neutral with sodium acetate or hydrochloric acid solution, adding a conditioning buffer solution, diluting with water to a reticle, shifting into a polyethylene cup, placing a plastic stirrer, inserting an electrode, continuously stirring the solution, and reading the potential value while continuously stirring the solution when the potential becomes stabilized, fully washing the electrode with water each time before measurement, absorbing to remove water by the filter paper, searching in a standard curve to obtain the fluoride concentration in a test solution according to the measured value of millivolts, and calculating the fluoride content according to the dilution ratio of the water sample. The method is simple and convenient in measuring process, and accurate in measurement result. Based on the method, people can trustingly drink the tested drinking water, so that the health of people is ensured.
Owner:曾成富

Compound traditional Chinese medicinal diet with diuresis promoting and calculus removing effects and preparation method thereof

The invention discloses a compound traditional Chinese medicinal diet with diuresis promoting and calculus removing effects and a preparation method thereof. The compound traditional Chinese medicinal diet is prepared from 28-30 g of coix seeds, 18-20 g of poria cocos, 28-30 g of lygodium japonicum, 4.35-4.55 g of potassium citrate monohydrate, 3.95-4.15 g of sodium citrate dihydrate and 0.07-0.08 g of anhydrous citric acid. The preparation method comprises the following steps: step 1, weighing 28-30 g of coix seeds and 18-20 g of poria cocos, weighing 28-30 g of lygodium japonicum, and putting the weighed lygodium japonicum into a 180-200-mesh filter bag; step 2, putting the materials weighed in the step 1 into a container; (3) adding water into the container in the step (2), heating until boiling, heating for 45-60 minutes at low power, and taking out the filter bag filled with the lygodium japonicum; 4, 4.35 g to 4.55 g of potassium citrate monohydrate, 3.95 g to 4.15 g of sodium citrate dihydrate and 0.07 g to 0.08 g of anhydrous citric acid are weighed and mixed with the mixed substance of the coix seeds, the poria cocos and the lygodium japonicum. The traditional Chinese medicine composition relieves the occurrence and development of urinary calculus from two aspects of diuresis and calculus removal, and has a good calculus dissolving effect; the food can be compounded into various edible forms, and is convenient to carry, good in taste and convenient to accept.
Owner:THE AFFILIATED HOSPITAL OF QINGDAO UNIV

High-load platinum-nickel ordered intermetallic compound and its preparation method and use

The invention provides a high-load platinum and nickel ordered intermetallic compound. The high-load platinum and nickel ordered intermetallic compound takes three-dimensional porous carbon gel as a carrier, and is prepared by a method comprising the following steps: evenly mixing graphene oxide-containing carbon carrier precursor dispersion liquid, a metal precursor solution containing a Pt precursor and an Ni precursor, a reducing agent and sodium citrate dehydrate; then, carrying out a hydrothermal reaction to generate high-load platinum and nickel disordered alloy evenly loaded in carbon gel; after that, carrying out heat treatment under the reducing atmosphere to form the high-load platinum and nickel ordered intermetallic compound evenly loaded in the carbon gel. Compared with the traditional high-load Pt / C catalyst, the catalyst provided by the invention relatively reduces the consumption of precious metal Pt; the activity of the catalyst is improved by using an intermetallic synergistic effect, the stability of the catalyst is improved by using high dispersion of ordered metal nanoparticles, and the high dispersion characteristic of the catalyst is still maintained after ordered heat treatment is carried out on the catalyst. The invention also discloses the preparation method of the high-load platinum and nickel ordered intermetallic compound. The invention also discloses use of the high-load platinum and nickel ordered intermetallic compound.
Owner:SHANGHAI ADVANCED RES INST CHINESE ACADEMY OF SCI

A kind of stable fasudil hydrochloride injection and preparation method thereof

The invention belongs to the field of pharmaceutical preparation, and particularly relates to stable fasudil hydrochloride injection and a preparation method thereof. The fasudil hydrochloride injection comprises fasudil hydrochloride, stabilizers, anhydrous citric acid, sodium citrate dihydrate, sodium chloride and water for injection, wherein the stabilizers comprise N-carboxymethyl chitosan and reduced glutathione according to the mass ratio of 1:(0.05-0.35). The preparation method includes the steps: dissolving components in the formula by the water for injection after pyrogen removal; adjusting pH (potential of hydrogen); adding medicinal carbon for stirring adsorption to further remove pyrogen and perform discoloration; performing filtration and decarburization; performing filtration, sterilization, sub-package, potting and sterilization to obtain the fasudil hydrochloride injection. The fasudil hydrochloride injection has fine light stability and simple in formula, insoluble particles are effectively suppressed, the preparation process is easily operated, and industrialization is facilitated.
Owner:中润药业有限公司
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