High-temperature-resistant UV polymeric bulk foam damping material and preparation method thereof

A technology of body foaming and damping materials, applied in the field of damping materials, can solve the problems of comprehensive performance and service life of materials, complicated and complicated process technology routes, and low temperature of damping materials, and achieves good energy absorption capacity and good flexibility. , the effect of strong chain activity

Active Publication Date: 2019-06-11
GUANGXI UNIV
View PDF9 Cites 1 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although the damping material prepared by this patent can solve the above problems to a certain extent, there are still the following disadvantages: 1. The technical route of this patent is very cumbersome and complicated, and the time and labor costs are high; 2. The damping performance of the material prepared by this patent It largely depends on the dispersion characteristics of inorganic particles. The inorganic particles used must first be treated with a silane coupling agent of a specific structure, otherwise they are easily precipitated from the system, or even agglomerated to cause serious phase separation. The service life is seriously affected; 3. The damping material prepared by this patent has a low service temperature, and the heat-resistant temperature is generally lower than 300°C, which cannot meet the use requirements of higher temperatures

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • High-temperature-resistant UV polymeric bulk foam damping material and preparation method thereof
  • High-temperature-resistant UV polymeric bulk foam damping material and preparation method thereof
  • High-temperature-resistant UV polymeric bulk foam damping material and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0038] The present invention also provides a method for preparing a high temperature resistant UV polymerization type body foam damping material, which comprises the following steps:

[0039] 1) Add POSS, acrylate copolymer, reactive diluent and photoinitiator to the reaction kettle, and continuously stir and swell at room temperature to form a uniform UV polymerized bulk foam damping material composition;

[0040] 2) Apply the UV polymerizable body foam damping material composition obtained in step 1) evenly on the release PET film, and irradiate it under ultraviolet light for 3-6 minutes to obtain the UV polymerizable body foam damping material .

Embodiment 1

[0042] A kind of preparation method of UV polymerization type bulk foam damping material, it comprises the following steps:

[0043] 1) Take each component by the following parts by weight:

[0044] Acrylate copolymer: 25 parts;

[0045] Active diluent: 69.5 parts;

[0046] Photoinitiator: 0.5 part;

[0047] POSS: 5 copies;

[0048] Described acrylate copolymer is the copolymer of epoxy acrylate and polyurethane acrylate, and its structure is as shown in formula (I):

[0049]

[0050] Wherein, the reactive diluent is a mixture of isooctyl acrylate and vinyl acetate in a mass ratio of 2:1, and the photoinitiator is 2,4,6-trimethylbenzoyl-diphenylphosphine oxide.

[0051] 2) Add POSS, acrylate copolymer, reactive diluent and photoinitiator to the reaction kettle, and continuously stir and swell at room temperature to form a uniform UV polymerized bulk foam damping material composition;

[0052] 3) Uniformly coat the UV polymerization type body foaming damping material co...

Embodiment 2

[0054] A kind of preparation method of UV polymerization type bulk foam damping material, it comprises the following steps:

[0055] 1) Take each component by the following parts by weight:

[0056] Acrylate copolymer: 30 parts;

[0057] Active diluent: 63.4 parts;

[0058] Photoinitiator: 0.6 part;

[0059] POSS: 6 copies;

[0060] Described linear acrylate copolymer is the copolymer of epoxy acrylate and polyurethane acrylate, and its structure is as shown in formula (I):

[0061]

[0062] Wherein, the reactive diluent is a mixture of styrene and vinyl acetate in a mass ratio of 2:1, and the photoinitiator is benzoylformate.

[0063] 2) Add POSS, acrylate copolymer, reactive diluent and photoinitiator to the reaction kettle, and continuously stir and swell at room temperature to form a uniform UV polymerized bulk foam damping material composition;

[0064] 3) Uniformly coat the UV polymerization type body foaming damping material composition obtained in step 2) on th...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
softening pointaaaaaaaaaa
Damping temperature rangeaaaaaaaaaa
thicknessaaaaaaaaaa
Login to view more

Abstract

The invention relates to a high-temperature-resistant UV polymericbulk foam damping material and a preparation method thereof. The preparation comprises the following steps: adding POSS, an acrylate copolymer, a reactive diluent and a photoinitiator into a reaction kettle, and performing stirring for swelling to form a uniform UV polymeric bulk foam damping material composition; and uniformly coating a release PET film by the obtained damping material composition, and performing illumination under ultraviolet light for 3-6 min to obtain the UV polymeric bulk foam damping material. The dampingmaterial provided by the invention has the following beneficial effects: 1, POSS is used as an inorganic bulk foaming agent, an addition amount of the POSS particles is controlled, so that the productdensity can be precisely controlled according to requirements, and the loss factor of the material can be improved; and the POSS can form stable nano-scale dispersion without any treatment in the material system; and 2, the process flow is simple, the reaction speed is fast, the production efficiency is high, and the costs are reduced.

Description

technical field [0001] The invention relates to the field of damping materials, in particular to a high-temperature-resistant UV polymerized bulk foaming damping material and a preparation method thereof. Background technique [0002] The vibration and noise generated by mechanical operation not only pollute the environment, but also affect the machining accuracy and product quality of the machine, accelerate the fatigue damage of the mechanical structure, and shorten the service life of the machine. Damping material is a material that converts solid mechanical vibration energy into heat energy and dissipates it. It is mainly used for vibration and noise control. The design principle of the damping material is: try to make the hysteresis loss as large as possible, the loss modulus is high, the storage modulus is low, and the effective damping temperature range is wide. The damping performance of a damping material can be measured in terms of its ability to dissipate vibrati...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Applications(China)
IPC IPC(8): C08L33/14C08L83/08C08J9/04
Inventor 赵辉黄崇杏刘杨王双飞黄丽婕赵思琪
Owner GUANGXI UNIV
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products