Preparation method of special dispersion PTFE oleo-resin for thread seal tape
The technology of raw material tape and resin is applied in the field of preparation of special dispersed PTFE oil-containing resin for raw material tape, which can solve the problems of uniformity, compatibility and instability, achieve uniform molecular weight distribution, good compatibility, and improve tensile properties. Effect
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Embodiment 1
[0014] ⑴Add 65L of water and 3.5kg of liquid paraffin to a 100L reactor, pump it out for replacement, control the temperature at 50°C, then add tetrafluoroethylene to the reactor, adjust the pressure to 2.0MPa and maintain it throughout.
[0015] (2) Add 7.4g of ammonium persulfate, 15g of succinic acid, and 120g of perfluoropolyether ammonium carboxylate into the reactor in step (1) with a metering pump;
[0016] (3) With a metering pump, 1.48L of sodium bisulfite solution with a mass percentage concentration of 1% is continuously added to step (1) reactor;
[0017] ⑷ When the gas mass flow meter shows 7kg, add 80g of perfluoropolyether ammonium carboxylate solution into the reaction kettle with a metering pump;
[0018] (5) Terminate the reaction after adding the sodium bisulfite solution;
[0019] (6) Add 25L of graphite dispersion with a mass percentage concentration of 10% (the present invention provides a method rather than a specific filler, graphite is used as an exam...
Embodiment 2
[0024] Change the graphite dispersion liquid described in step (6) into titanium dioxide dispersion liquid in embodiment 1, and other operations are the same as embodiment 1.
[0025] The raw material tape finally prepared in this example has a uniform appearance and color, no defect points, no color fading after rubbing, and no abnormality in the tensile data.
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