Method for preparing soft and hard movable compound bone rehabilitation protection tool through 3D printing
A 3D printing and bone rehabilitation technology, applied in the field of 3D printing, can solve the problem that it is difficult to match the active parts of the joints with the patient, and achieve the effect of improving the treatment effect and broad-spectrum antibacterial effect
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Embodiment 1
[0031] The preparation of embodiment 1 antibacterial nylon material
[0032] The preparation method of the described antibacterial nylon material is: mix the raw materials of nylon 6, calcium carbonate, chopped glass fiber, coupling agent, lubricant, antioxidant and antibacterial agent according to the following parts by weight, and then carry out Get it by extrusion granulation;
[0033] The described raw material parts by weight consist of: 100 parts of nylon 6; 10 parts of calcium carbonate; 8 parts of chopped glass fiber; 2 parts of coupling agent vinyltrimethoxysilane; 2 parts of lubricant calcium stearate; 1 part of triethylene glycol ether-di(3-tert-butyl-4-hydroxy-5-methylphenyl) propionate; 1 part of antibacterial agent;
[0034] The antibacterial agent is prepared by the following method: soaking the nano-silver in an aqueous ethanol solution containing a 70% volume fraction of the Cortex ditsifolia extract for 12 hours, and then concentrating and drying the aqueous...
Embodiment 2
[0035] The preparation of embodiment 2 antibacterial nylon materials
[0036] The preparation method of the described antibacterial nylon material is: mix the raw materials of nylon 6, calcium carbonate, chopped glass fiber, coupling agent, lubricant, antioxidant and antibacterial agent according to the following parts by weight, and then carry out Get it by extrusion granulation;
[0037] The described raw material parts by weight consist of: 100 parts of nylon 6; 10 parts of calcium carbonate; 8 parts of chopped glass fiber; 2 parts of coupling agent vinyltrimethoxysilane; 2 parts of lubricant calcium stearate; 1 part of triethylene glycol ether-di(3-tert-butyl-4-hydroxy-5-methylphenyl) propionate; 1 part of antibacterial agent;
[0038] The antibacterial agent is prepared by the following method: soaking the nano-silver in an aqueous ethanol solution containing a 70% volume fraction of the Cortex ditsifolia extract for 12 hours, and then concentrating and drying the aqueou...
experiment example 1
[0052] Antibacterial performance test of experimental example 1 antibacterial nylon material
[0053] The antibacterial nylon materials prepared in Examples 1-2 and Comparative Examples 1-2 were printed into test specimens with a 3D printer. Refer to the method in GB / T 31402-2015 to test the antibacterial effect of antibacterial nylon materials, and calculate the bacteriostatic rate; bacteriostatic rate = (the number of bacteria after 24 hours of inoculation without antibacterial treatment - the number of bacteria after 24 hours of inoculation with antibacterial treatment number) / the number of bacteria after 24 hours of inoculation without antibacterial treatment; the test results are shown in Table 1.
[0054] Table 1. Antibacterial performance test results of antibacterial nylon materials
[0055] Escherichia coli inhibition rate Staphylococcus antibacterial rate MRSA inhibition rate Embodiment 1 antibacterial nylon material 99.98% 99.99% 74.41% ...
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