Core-shell capsule for reducing harmful components of mainstream smoke and preparation and application of core-shell capsule
A technology of harmful components and mainstream smoke, applied in the field of the tobacco industry, can solve the problems of harm reduction or aroma enhancement effect of cigarettes, inability to realize the industrial application of cigarettes, loss of harm reduction effect, etc., and achieve good harm reduction characteristics and controllable size. , particle size controllable effect
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Embodiment 1
[0073] Weigh 12g of polyvinyl alcohol and dissolve it in 400mL of deionized water at 80°C to obtain a polyvinyl alcohol solution.
[0074] Weigh 3.6g of polylactic acid particles and dissolve in 30mL of dichloromethane to obtain a polylactic acid solution.
[0075] The polylactic acid solution and deionized water were put into syringes respectively, placed on two syringe pumps, connected to the coaxial double-needle reactor, and the flow rates of the two syringe pumps were 5mL / L (water) and 6mL / L (poly Lactic acid solution) was dropped into the polyvinyl alcohol solution, mechanically stirred for 6 hours at a stirring speed of 250r / min, the product was filtered under reduced pressure, washed with deionized water, and then collected to obtain water-in-polylactic acid capsules. The particle diameter that measures water-packed capsule is 3.5mm (see image 3 -a).
Embodiment 2
[0077] Compared with Example 1, the main difference is that the PLA solubility of the wall material solution is 0.15g / mL; details are as follows:
[0078] Weigh 12g of polyvinyl alcohol and dissolve it in 400mL of deionized water at 80°C to obtain a polyvinyl alcohol solution.
[0079] Weigh 4.5g of polylactic acid particles and dissolve in 30mL of dichloromethane to obtain a polylactic acid solution.
[0080] The polylactic acid solution and deionized water were put into syringes respectively, placed on two syringe pumps, connected to the coaxial double-needle reactor, and the flow rates of the two syringe pumps were 5mL / L (water) and 6mL / L (poly Lactic acid solution) was dropped into the polyvinyl alcohol solution, mechanically stirred for 6 hours at a stirring speed of 250r / min, the product was filtered under reduced pressure, washed with deionized water, and then collected to obtain water-in-polylactic acid capsules. The particle diameter of water-packed capsule is about ...
Embodiment 3
[0082] Compared with Example 1, the main difference is that the PLA solubility of the wall material solution is 0.2g / mL, and the flow ratio of the core material solution / wall material solution is 1:1.6; details are as follows:
[0083] Weigh 12g of polyvinyl alcohol and dissolve it in 400mL of deionized water at 80°C to obtain a polyvinyl alcohol solution.
[0084] Weigh 6g of polylactic acid particles and dissolve in 30mL of dichloromethane to obtain a polylactic acid solution.
[0085] Put the polylactic acid solution and deionized water into syringes respectively, place them on two syringe pumps, connect the coaxial double-needle reactor, and the flow rates of the two syringe pumps are 5mL / h (water flow rate) and 8mL / h respectively. (Flow rate of polylactic acid solution), drop into polyvinyl alcohol solution, mechanically stir for 6h, stirring speed is 250r / min, the product is vacuum filtered, washed with deionized water, and then collected to obtain polylactic acid water-...
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