Preparation method of carbon fiber reinforced aluminum-based composite material
A technology for strengthening aluminum-based and composite materials, applied in the field of composite materials, can solve the problems of difficult industrialization, complicated preparation process, small thermal expansion coefficient, etc., and achieve the effects of avoiding black core phenomenon, simple preparation process and low production cost
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[0033] A method for preparing a carbon fiber reinforced aluminum matrix composite material of the present invention comprises the following steps:
[0034] S1. Put the carbon fiber in a muffle furnace and heat it up to 350-500°C for 10-80 minutes, then put the burned carbon fiber into ammonium persulfate with a concentration of 100-200g / L and a concentration of 50-200g / L at room temperature. 100ml / L H 2 SO 4 In the mixed solution, roughen treatment for 10-60 minutes;
[0035] S2. Add the roughened carbon fiber to 5-30g / L SnCl 2 Add a small amount of HCl at a concentration of 20-45g / L for sensitization treatment for 1-10min, then take it out and rinse it in still water for 3-20min, add the rinsed carbon fiber to 1-10g / L silver nitrate and 5-20ml / L Ammonia water mixture was activated at room temperature for 5-20 minutes;
[0036] S3. Put the activated carbon fiber into the chemical plating solution, control the temperature at 10-30°C and control the time for 10-60 minutes, a...
Embodiment 1
[0041] A method for preparing a carbon fiber reinforced aluminum matrix composite material of the present invention comprises the following steps:
[0042] S1. Put the carbon fiber in a muffle furnace and heat it up to 350°C for 10 minutes, then put the burned carbon fiber into ammonium persulfate with a concentration of 100g / L and H at a concentration of 50ml / L at room temperature. 2 SO4 In the mixed solution, roughen for 10 minutes;
[0043] S2, the carbon fiber of roughening treatment is added to the SnCl of 5g / L 2 Add a small amount of HCl at a concentration of 20g / L for sensitization treatment for 1min, then take it out and rinse it in still water for 3min, add the rinsed carbon fiber to a mixture of 1g / L silver nitrate and 5ml / L ammonia water for 5min at room temperature;
[0044] S3. Put the activated carbon fiber into the chemical plating solution, control the temperature at 10°C and control the time for 10 minutes, and keep stirring to complete the chemical plating. ...
Embodiment 2
[0048] A method for preparing a carbon fiber reinforced aluminum matrix composite material of the present invention comprises the following steps:
[0049] S1. Put the carbon fiber in a muffle furnace and heat it up to 400°C for 30 minutes, then put the burned carbon fiber into ammonium persulfate with a concentration of 140g / L and H with a concentration of 70ml / L at room temperature. 2 SO 4 In the mixed solution, roughen for 20 minutes;
[0050] S2, the carbon fiber of coarsening treatment is added to the SnCl of 10g / L 2 Add a small amount of HCl at a concentration of 25g / L for sensitization treatment for 4min, then take it out and rinse it in still water for 8min, add the rinsed carbon fiber to a mixture of 4g / L silver nitrate and 8ml / L ammonia water for 8min activation at room temperature;
[0051] S3. Put the activated carbon fiber into the chemical plating solution, control the temperature at 15°C and control the time for 20 minutes, and keep stirring to complete the ch...
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