Preparation method of built-in nasal cavity polyurethane filtering material with antibacterial function
A filter material, polyurethane technology, applied in the field of woven fiber materials, can solve the problems of strong human discomfort, inconvenient wearing, complicated process, etc., and achieve the effect of enhancing interpersonal communication and communication, avoiding stimulation, and convenient use
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Embodiment 1
[0028] A preparation method of a built-in nasal cavity polyurethane filter material with antibacterial function, comprising the following steps:
[0029] (1) Dehydrate the mixture of 0.05 mole polyethylene glycol with a molecular weight of 3000 and 0.05 mole 1,4-butanediol at 120°C for 2 hours under reduced pressure, so that the water content in the mixture is below 0.05%, and cool down to 60°C Standby, mix and react with 0.105 moles of toluene diisocyanate (TDI) to prepare thermoplastic polyurethane elastomer, which is recorded as part A;
[0030] (2) Mix tetrahydrofuran and dimethylformamide with a water content of less than 0.05% at a mass ratio of 1:3, and record it as part B;
[0031] (3) Fully mix A and B according to the mass ratio of 1:8, stir evenly, and record it as part C;
[0032] (4) By mass, take 400 parts of C mixed solution, add 1 part of titanium dioxide-silver antibacterial agent, stir evenly and let it stand for 2 hours for defoaming to obtain spinning stoc...
Embodiment 2
[0037] A preparation method of a built-in nasal cavity polyurethane filter material with antibacterial function, comprising the following steps:
[0038] (1) Dehydrate the mixture of 0.05 mole polyethylene glycol with a molecular weight of 2000 and 0.05 mole 1,4-butanediol at 120°C for 2 hours under reduced pressure, so that the water content in the mixture is below 0.05%, and cool down to 60°C Standby, mix and react with 0.105 moles of phenylene diisocyanate (PPDI) to prepare thermoplastic polyurethane elastomer, which is recorded as part A;
[0039] (2) Mix tetrahydrofuran and dimethylformamide with a water content of less than 0.05% at a mass ratio of 1:3, and record it as part B;
[0040] (3) Fully mix A and B according to the mass ratio of 1:8, stir evenly, and record it as part C;
[0041] (4) In terms of mass, take 400 parts of C mixed solution, add 1 part of ε-polylysine, stir evenly and let it stand for 2 hours for degassing to obtain spinning stock solution;
[004...
Embodiment 3
[0045] A preparation method of a built-in nasal cavity polyurethane filter material with antibacterial function, comprising the following steps:
[0046] (1) Dehydrate the mixture of 0.05 mole polyethylene glycol with a molecular weight of 3000 and 0.05 mole 1,4-butanediol at 120°C for 2 hours under reduced pressure, so that the water content in the mixture is below 0.05%, and cool down to 60°C Standby, mix and react with 0.105 moles of diphenylmethane diisocyanate (MDI) to prepare thermoplastic polyurethane elastomer, denoted as part A;
[0047] (2) Mix tetrahydrofuran and dimethylformamide with a water content of less than 0.05% at a mass ratio of 1:3, and record it as part B;
[0048] (3) Fully mix A and B according to the mass ratio of 1:8, stir evenly, and record it as part C;
[0049] (4) In terms of mass, take 400 parts of C mixed solution, add 1 part of trichlorodiphenylurea, stir evenly and let it stand for 2 hours for defoaming to obtain spinning stock solution;
[0...
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