Preparation method of organosilicone modified phenolic aerogel
A technology of organosilicon and airgel, which is applied in the field of airgel heat insulation research, can solve the problems of poor environmental protection and cumbersome preparation methods, and achieve the effects of simple method, easy-to-obtain catalyst, and reduced preparation time
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specific Embodiment approach 1
[0020] Specific embodiment one: what this embodiment records is a kind of preparation method of organosilicon modified phenolic airgel, described method is:
[0021] Mix phenols, aldehydes, and silicones in proportion, the molar ratio of phenols to aldehydes is 1:1.4~2, the molar ratio of phenols to silicones is 1:0~2, add water to make the mass fraction 20% to 40% solution, stirred for 30 to 90 minutes, adding acid and alkali, controlling the pH value of the solution to 3.5 to 6.5, raising the temperature to solidify the silicone phenolic formaldehyde, and drying under normal pressure to obtain the silicone modified phenolic formaldehyde aerogel.
specific Embodiment approach 2
[0022] Specific embodiment two: the preparation method of a kind of organosilicon modified phenolic aerogel described in specific embodiment one, described phenol is a kind of in phenol, resorcinol or pyrocatechol; The class is one of formaldehyde, acetaldehyde or furfural.
specific Embodiment approach 3
[0023] Specific embodiment three: the preparation method of a kind of organosilicon modified phenolic airgel described in specific embodiment one, described acid is a kind of in hydrochloric acid, sulfuric acid, nitric acid or acetic acid, and described alkali is sodium carbonate, carbonic acid One of sodium hydrogen, ammonia or triethylamine.
[0024] Specific embodiment four: the preparation method of a kind of organosilicon modified phenolic airgel described in specific embodiment one, described organosilicon is methyltrimethoxysilane, methyltriethoxysilane, ethyltrimethoxysilane dimethylsilane, dimethyldimethoxysilane, dimethyldiethoxysilane, methyltripropoxysilane, dimethyldipropoxysilane, ethyltrimethoxysilane, diethyldimethylsilane Oxysilane, Ethyltriethoxysilane, Diethyldiethoxysilane, Propyltrimethoxysilane, Dipropyldimethoxysilane, Propyltriethoxysilane or Dipropyldiethylsilane One or more mixtures of oxysilanes.
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