Antiseptic system for infant wet tissue immersion liquid and preparation method thereof
A technology of baby wipes and soaking liquid, which is applied in the field of antibacterial sanitary products, can solve the problems of low safety, toxic and side effects, bad sour taste, etc., and achieve the effect of broad market prospects, high safety performance, and wide spectrum of antiseptic bacteria
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Embodiment 1
[0031] A kind of preservative system used for soaking liquid of baby wipes, comprising the following components by weight ratio: ε-polylysine 0.05%, lauroyl arginine ethyl ester hydrochloride 0.08%, natamycin 0.01%, Dehydroacetic acid 0.01%, lactic acid 0.01%, alkyl glycoside 0.1%, glycerin 0.2%, secondary reverse osmosis water 99.54%.
[0032] The lauroyl arginine ethyl ester hydrochloride is fully reacted by L-arginine hydrochloride in a mixed solution of water and methyl ethyl ketone with lauroyl chloride at a pH of 7 and a temperature of -5°C. After the reaction is completed, adjust the pH to 5, centrifuge, and dry to obtain lauroyl arginine, then add ethanol and thionyl chloride to the lauroyl arginine to fully react, dry to obtain lauroyl arginine ethyl ester hydrochloride The crude product is obtained by adding ethyl acetate to the crude product of ethyl lauroyl arginine hydrochloride, stirring, dissolving, adjusting the pH to 5, standing still, taking the organic layer...
Embodiment 2
[0053] A preservative system for soaking liquid of baby wet wipes, comprising the following components by weight ratio: ε-polylysine 0.275%, lauroyl arginine ethyl ester hydrochloride 0.24%, natamycin 0.055%, Dehydroacetic acid 0.03%, lactic acid 0.055%, alkyl glycoside 0.3%, glycerin 0.5%, secondary reverse osmosis water 98.545%.
[0054] The lauroyl arginine ethyl ester hydrochloride is fully reacted by L-arginine hydrochloride in a mixed solution of water and ethyl acetate and lauroyl chloride at a pH of 10 and a temperature of 12°C. After the reaction is completed, adjust the pH to 7, centrifuge, and dry to obtain lauroyl arginine, then add ethanol and thionyl chloride to the lauroyl arginine to fully react, dry to obtain lauroyl arginine ethyl ester hydrochloride The crude product is obtained by adding butyl acetate to the crude product of ethyl lauroyl arginine hydrochloride, stirring, dissolving, adjusting the pH to 6, standing still, taking the organic layer, cooling t...
Embodiment 3
[0074] A kind of preservative system used for soaking liquid of baby wipes, comprising the following components by weight ratio: ε-polylysine 0.5%, lauroyl arginine ethyl ester hydrochloride 0.4%, natamycin 0.1%, Dehydroacetic acid 0.05%, lactic acid 0.1%, alkyl glycoside 0.5%, glycerin 0.8%, secondary reverse osmosis water 97.55%.
[0075] The lauroyl arginine ethyl ester hydrochloride is fully reacted by L-arginine hydrochloride in a mixed solution of water and butyl acetate and lauroyl chloride at a pH of 12 and a temperature of 30°C. After the reaction is completed, adjust the pH to 9, centrifuge, and dry to obtain lauroyl arginine, then add ethanol and thionyl chloride to the lauroyl arginine to fully react, dry to obtain lauroyl arginine ethyl ester hydrochloride The crude product is obtained by adding ethyl acetate to the crude product of ethyl lauroyl arginine hydrochloride, stirring, dissolving, adjusting the pH to 7, standing still, taking the organic layer, cooling ...
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