A p-type delafossite structure cusco 2 Crystal material and its preparation method and use
A technology of crystal material and delafossite, which is applied in the field of p-type delafossite structure CuScO2 crystal material and its preparation, can solve the problems of less crystal powder material preparation and performance research
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Embodiment 1
[0031] This embodiment provides an electrolytic water oxygen evolution catalyst delafossite structure CuScO 2 A crystal material and a preparation method thereof, comprising the steps of:
[0032] First prepare the reaction precursor (or hydrothermal reaction precursor): the Cu(NO 3 ) 2 and Sc(NO 3 ) 3 According to the molar ratio of 1:1, add to the reaction solution, stir with a magnetic stirrer for 10 to 15 minutes to dissolve, then add Cu(NO 3 ) 2 NaOH with 10 times the molar number is used as a mineralizer, and finally 0.5 ml of ethylene glycol is added, and the stirring is continued for 10 to 15 minutes until it is completely dissolved to obtain a reaction precursor.
[0033] The above reaction precursor was transferred to a hydrothermal reactor (generally polytetrafluoroethylene), the resistivity of deionized water was 18.24MΩ·cm (25°C), and the filling rate was about 70%. After sealing the kettle body, place it in a programmed temperature-controlled oven for hydro...
Embodiment 2
[0036] This embodiment provides an electrolytic water oxygen evolution catalyst delafossite structure CuScO 2 A crystal material and a preparation method thereof, comprising the steps of:
[0037] First prepare the reaction precursor (or hydrothermal reaction precursor): the Cu(NO 3 ) 2 and Sc(NO 3 ) 3 According to the molar ratio of 1.5:1, add to the reaction solution, stir for 10 to 15 minutes with a magnetic stirrer to dissolve, then add Cu(NO 3 ) 2 NaOH with 10 times the number of moles is used as a mineralizer, and finally 1.0 ml of ethylene glycol is added, and the stirring is continued for 10 to 15 minutes until it is completely dissolved to obtain a reaction precursor.
[0038] The above reaction precursor was transferred to a hydrothermal reactor (generally polytetrafluoroethylene), the resistivity of deionized water was 18.24MΩ·cm (25°C), and the filling rate was about 65%. After sealing the kettle body, place it in a programmed temperature-controlled oven for ...
Embodiment 3
[0041] This embodiment provides an electrolytic water oxygen evolution catalyst delafossite structure CuScO 2 A crystal material and a preparation method thereof, comprising the steps of:
[0042] First prepare the reaction precursor (or hydrothermal reaction precursor): the Cu(NO 3 ) 2 and Sc(NO 3 ) 3 According to the molar ratio of 1.25:1, add to the reaction solution, stir with a magnetic stirrer for 10 to 15 minutes to dissolve, then add Cu(NO 3 ) 2 NaOH with 6 times the molar number is used as a mineralizer, and finally 1.0 ml of ethylene glycol is added, and the stirring is continued for 10 to 15 minutes until it is completely dissolved to obtain a reaction precursor.
[0043] The above reaction precursor was transferred to a hydrothermal reactor (generally polytetrafluoroethylene), the deionized water resistivity was 18.24MΩ·cm (25°C), and the filling rate was about 75%. After sealing the kettle body, place it in a programmed temperature-controlled oven for hydrot...
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