Preparation method of ultra-fine-crystal high-toughness heat-resistant aluminum alloy lead
A technology of aluminum alloy wire and ultra-fine grain, which is applied in the direction of cable/conductor manufacturing, electrical components, circuits, etc., and can solve the problems of affecting the conductivity of materials, easy oxidation, and the inability to ensure the uniformity and density of materials.
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[0012] The invention is a method for preparing an ultra-fine-grained, high-strength and tough heat-resistant aluminum alloy wire, the steps of which are as follows:
[0013] (1) Ingredients: It is composed of the following components by weight: 100 parts of industrial pure aluminum, 0.7 parts of aluminum-zirconium alloy, 0.4 part of aluminum-copper alloy, 0.4 part of aluminum-erbium alloy, 0.0015 parts of refiner Al-5Ti-B, metamorphic Agent Sr 0.06 parts, refining agent hexachloroethane 0.5 parts;
[0014] (2) Melting: Add pure aluminum to a coreless intermediate frequency induction furnace, raise the temperature of the furnace to 740°C, and start ultrasonic vibration for 20s when the temperature reaches 720°C. agent and refiner, electromagnetic stirring is carried out during this period, and then refining and slag removal are started;
[0015] (3) The prepared alloy liquid is cast into an ingot, and then the alloy ingot is subjected to multidirectional forging, homogenizatio...
Embodiment 1
[0031] Embodiment 1: The present invention is a method for preparing an ultra-fine-grained, high-strength, heat-resistant aluminum alloy wire, the steps of which are:
[0032] Step (1) Prepare materials: industrial pure aluminum (99.99%), AI-Er (Er: 12.61% Si: 0.013% Fe: 0.051% Ca: 0.0048%) master alloy, AI-Cu (Cu: 51.96% Si: 0.013% Fe: 0.018% Ca: 0.0025%) master alloy, Al-Zr (Zr: 10.60%) master alloy and Al-5Ti-B refiner Sr modifier, hexachloroethane refining agent.
[0033] Step (2) First, preheat the charge in an oven at 210°C to 220°C for 30 minutes to fully dry it, melt it in a white corundum crucible at a melting temperature of 750°C, stir and remove slag, then measure the temperature, and add the master alloy at 740°C , Stir for 30s, shake for 30s. Keep warm for 3 minutes, add refining agent after temperature measurement, shake for 30 seconds, remove slag, and open the incubator. When the temperature drops to 725°C, it is poured into a copper mold. Apply the prepared...
Embodiment 2
[0050] The difference between this embodiment and Embodiment 1 is that the mold angle used in step (10) is 120°.
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