Nitrogen-doped molybdenum disulfide/graphene composite material
A technology of molybdenum disulfide and composite materials, applied in electrical components, battery electrodes, circuits, etc., can solve the problems of low nitrogen doping content of nitrogen-doped precursors, difficulty in obtaining raw materials, complicated and time-consuming operations, etc., and achieve large specific surface area , good stability, and the effect of simplifying the production process
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Embodiment 1
[0038] (1) Weigh 1.0g of graphene oxide and disperse it in 20mL of 37% formaldehyde aqueous solution, place it in an ultrasonic instrument and disperse evenly, record it as dispersion A.
[0039] (2) Weigh 3.0g of melamine and 5.0g of ammonium tetrathiomolybdate and add them into 40mL of deionized water, place them in an ultrasonic instrument and ultrasonically disperse evenly, and record it as dispersion liquid B.
[0040] (3) Mix Dispersion A and Dispersion B, raise the temperature of the water bath to 60°C and stir for 10 minutes. Then triethanolamine was added to the reaction solution to adjust the pH value of the reaction solution system to 8.0, and the mixture was uniformly mixed by ultrasonic, then the reaction solution was poured into a high-pressure reactor, and the temperature was raised to 120° C. for 12 hours to react. Suction filtration, vacuum drying to obtain a black solid powder.
[0041] (4) Put the black solid powder obtained in step (3) into a microwave rea...
Embodiment 2
[0043] (1) Weigh 1.0g graphene oxide and disperse it in 30mL 37% formaldehyde aqueous solution, place it in an ultrasonic instrument and disperse evenly, record it as dispersion liquid A.
[0044] (2) Weigh 5.0g of melamine and 8.0g of ammonium tetrathiomolybdate and add them into 40mL of deionized water, place them in an ultrasonic instrument and ultrasonically disperse evenly, and record it as dispersion liquid B.
[0045] (3) Mix Dispersion A and Dispersion B, raise the temperature of the water bath to 60°C and stir for 10 minutes. Then triethanolamine was added to the reaction solution to adjust the pH value of the reaction solution system to 8.0, and the mixture was uniformly mixed by ultrasonic, then the reaction solution was poured into a high-pressure reactor, and the temperature was raised to 120° C. for 12 hours to react. Suction filtration, vacuum drying to obtain a black solid powder.
[0046] (4) Put the black solid powder obtained in step (3) into a microwave re...
Embodiment 3
[0048] (1) Weigh 1.0g graphene oxide and disperse it in 30mL 37% formaldehyde aqueous solution, place it in an ultrasonic instrument and disperse evenly, record it as dispersion liquid A.
[0049] (2) Weigh 10.0g of melamine and 10.0g of ammonium tetrathiomolybdate and add them into 40mL of deionized water, place them in an ultrasonic apparatus and ultrasonically disperse evenly, and record it as dispersion liquid B.
[0050] (3) Mix Dispersion A and Dispersion B, raise the temperature of the water bath to 70°C and stir for 10 minutes. Then triethanolamine was added to the reaction solution to adjust the pH value of the reaction solution system to 8.0, and the mixture was uniformly mixed by ultrasonic, then the reaction solution was poured into a high-pressure reactor, and the temperature was raised to 120° C. for 12 hours to react. Suction filtration, vacuum drying to obtain a black solid powder.
[0051] (4) Put the black solid powder obtained in step (3) into a microwave r...
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