Preparation method of high-strength thermal insulation concrete plate
A heat-insulating concrete, high-strength technology, applied in the field of building materials, can solve problems such as low strength, and achieve the effects of high mechanical strength, stable structure and complete shape
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Embodiment 1
[0032] In parts by weight, weigh 20 parts of desulfurized gypsum, 12 parts of glycerin, and 120 parts of deionized water respectively, add desulfurized gypsum and glycerin into deionized water, and stir at 300 r / min for 40 minutes at room temperature to obtain gypsum Suspension, put the gypsum suspension in a high-temperature and high-pressure reactor, stir and react at a speed of 160r / min for 2 hours under the conditions of a temperature of 200°C and a pressure of 20MPa to obtain a reaction slurry, and use 100°C deionized water to prepare the reaction slurry Wash 3 times, place in a centrifuge, centrifuge at 4000r / min for 12min at room temperature, take out the lower layer of solid, dry in an oven at 120°C for 2h, cool at room temperature to obtain gypsum whiskers;
[0033] Then in parts by weight, weigh 30 parts of glass microspheres, 120 parts of 10% sodium hydroxide solution by mass fraction, 1.2 parts of 3-aminopropyltriethoxysilane, 0.6 parts of N-octyltriethyl Oxysilane...
Embodiment 2
[0036] In parts by weight, weigh 25 parts of desulfurized gypsum, 15 parts of glycerol, and 150 parts of deionized water respectively, add desulfurized gypsum and glycerin into deionized water, and stir for 50 minutes at a speed of 325 r / min at room temperature to obtain gypsum Suspension, put the gypsum suspension in a high-temperature and high-pressure reactor, stir and react at a speed of 180r / min for 3h under the conditions of a temperature of 220°C and a pressure of 25MPa to obtain a reaction slurry, and use 100°C deionized water to prepare the reaction slurry Wash 4 times, place in a centrifuge, centrifuge at a speed of 4500r / min for 14min at room temperature, remove the lower layer of solid, dry in an oven at 140°C for 3h, and cool at room temperature to obtain gypsum whiskers;
[0037] Then in parts by weight, weigh 35 parts of glass microspheres, 140 parts of 10% sodium hydroxide solution by mass fraction, 1.4 parts of 3-aminopropyltriethoxysilane, 0.7 parts of N-octyl...
Embodiment 3
[0040] In parts by weight, weigh 30 parts of desulfurized gypsum, 18 parts of glycerin, and 180 parts of deionized water, add desulfurized gypsum and glycerin into deionized water, and stir at 350 r / min for 60 minutes at room temperature to obtain gypsum Suspension, put the gypsum suspension in a high-temperature and high-pressure reactor, stir and react at a speed of 200r / min for 4h under the conditions of a temperature of 240°C and a pressure of 30MPa, to obtain a reaction slurry, and use 100°C deionized water to prepare the reaction slurry Wash 5 times, place in a centrifuge, centrifuge at 5000r / min for 16min at room temperature, take out the lower layer of solid, dry in an oven at 160°C for 4h, cool at room temperature to obtain gypsum whiskers;
[0041] In parts by weight, weigh 40 parts of glass microspheres, 160 parts of 10% sodium hydroxide solution by mass fraction, 1.6 parts of 3-aminopropyltriethoxysilane, 0.8 parts of N-octyltriethoxy Base silane, 80 parts of absol...
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