Electret nanofiber filtering material and preparation method thereof
A nanofiber and filter material technology, which is applied in the field of electret nanofiber filter material and its preparation, can solve the problems of low filtration efficiency of fine particles and unstable electret performance, and achieve improved electrostatic effect, low production cost, and high performance retention The effect of stability
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Embodiment 1
[0032] This example 1 provides an electret nanofiber filter material in a preferred embodiment, which is prepared by loading the spinning solution on the support material of the PP melt-blown non-woven fabric through the electrospinning method. Wherein, the spinning solution in this embodiment comprises the following components by weight:
[0033] 13 parts polyacrylonitrile (PAN);
[0034] 3 parts methyl 2-aminothiophene-3-carboxylate; and
[0035] 84 parts of N,N-dimethylformamide solvent.
[0036] The present embodiment 1 also provides the preparation method of above-mentioned material, specifically as follows:
[0037] (1) Weigh 3 parts of methyl 2-aminothiophene-3-carboxylate and add it to a container containing 84 parts of N,N-dimethylformamide solvent, place the container in a water bath at 60°C and heat it. The mixture was stirred until dissolved, and then 13 parts of polyacrylonitrile (PAN) was weighed and added to the above thiophene solution to form a uniform tran...
Embodiment 2
[0050] Example 2 provides another preferred embodiment of the electret nanofiber filter material, which is prepared by loading the spinning solution on the PP spunbonded non-woven support material. In this embodiment, the spinning solution comprises the following components by weight:
[0051] 15 parts polyvinylidene fluoride (PVDF);
[0052] 4 parts 5-amino-2-thiophenecarbaldehyde; and
[0053] 81 parts of N,N-dimethylacetamide solvent.
[0054] The present embodiment also provides the preparation method of above-mentioned material, specifically as follows:
[0055] (1) Weigh 4 parts of 5-methoxy-2 thiophene carboxaldehyde and add it to a container containing 81 parts of N,N-dimethylacetamide solvent, heat the container in a water bath at 60°C, and Stir the mixture until dissolved, then weigh 15 parts of polyvinylidene fluoride (PVDF) and add it to the above thiophene solution to form a uniform and transparent spinning solution.
[0056] (2) Set the parameters of the elec...
Embodiment 3
[0067] This embodiment provides another preferred embodiment of the electret nanofiber filter material, which is prepared by loading the spinning solution on the PP melt-blown non-woven support material, and the spinning solution includes the following components by weight: Minute:
[0068] 22 parts polystyrene (PS);
[0069] 3 parts dimethyl 4-aminothiophene-2,3-dicarboxylate; and
[0070] 75 parts of N,N-dimethylacetamide solvent.
[0071] Present embodiment provides the preparation method of above-mentioned material simultaneously, specifically as follows:
[0072] (1) Weigh 3 parts of dimethyl 4-aminothiophene-2,3-dicarboxylate into a container containing 75 parts of N,N-dimethylacetamide solvent, and place the container in a 60°C water bath Heat and stir the mixture in the container until it dissolves, then weigh 22 parts of polystyrene (PS) and add it to the above thiophene solution to form a uniform transparent solution, that is, a spinning solution.
[0073] (2) Se...
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