Polyester filament yarn containing mint extract and preparation method thereof
A mint extract and polyester filament technology, applied in the field of spinning, can solve the problems of complex preparation process, affecting fiber quality, high production cost, etc., achieve high transparency, high comfort, and reduce the effect of bacterial adhesion
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Embodiment 1
[0028] Embodiment 1 A kind of polyester filament containing peppermint extract and preparation method thereof
[0029] 1. Preparation of SiO2 porous gel powder
[0030] First, weigh 10.5g tetraethyl orthosilicate, dissolve it in a mixed solvent of 12 times the weight, add 5 drops of ammonia water with a dropper, and heat it in a hot water bath at 65°C to hydrolyze the solution into transparent tetraethyl orthosilicate Sol, continue to keep warm, make tetraethyl silicate sol completely become gel; Finally, gel is placed in freeze-drying box, can obtain SiO2 porous gel powder;
[0031] Described mixed solvent is the mixed solvent of Virahol and deionized water, and the volume ratio of Virahol and water is 40 / 60;
[0032] For the freeze-drying, the vacuum degree is 0.04MPa, the temperature is set to -10°C, and the freeze-drying is carried out for 8 hours;
[0033] 2. Preparation of modified granules containing peppermint extract
[0034] Put the SiO2 porous gel powder in 1.0wt...
Embodiment 2
[0056] Embodiment 2 A kind of polyester filament containing peppermint extract and preparation method thereof
[0057] 1. Preparation of SiO2 porous gel powder
[0058] First weigh 11.8g tetraethyl orthosilicate, dissolve it in a mixed solvent 15 times the weight, add 8 drops of ammonia water with a dropper, and heat it in a hot water bath at 70°C to hydrolyze the solution into transparent tetraethyl orthosilicate Sol, continue to keep warm, make tetraethyl silicate sol completely become gel; Finally, gel is placed in freeze-drying box, can obtain SiO2 porous gel powder;
[0059] Described mixed solvent is the mixed solvent of Virahol and deionized water, and the volume ratio of Virahol and water is 50 / 50;
[0060] For the freeze-drying, the vacuum degree is 0.05MPa, the temperature is set to -10°C, and the freeze-drying is carried out for 8 hours;
[0061] 2. Preparation of modified granules containing peppermint extract
[0062] Put the SiO2 porous gel powder in 1.5wt% di...
Embodiment 3
[0084] Embodiment 3 A kind of polyester filament containing peppermint extract and preparation method thereof
[0085] 1. Preparation of SiO2 porous gel powder
[0086] First weigh 111.2g tetraethyl orthosilicate, dissolve it in a mixed solvent 12 times the weight, add 8 drops of ammonia water dropwise with a dropper, and heat it in a hot water bath at 70°C to hydrolyze the solution into transparent tetraethyl orthosilicate Sol, continue to keep warm, make tetraethyl orthosilicate sol become gel completely; Finally, gel is placed in freeze-drying box, can obtain SiO2 porous gel powder;
[0087] Described mixed solvent is the mixed solvent of Virahol and deionized water, and the volume ratio of Virahol and water is 45 / 55;
[0088] For the freeze-drying, the vacuum degree is 0.05MPa, the temperature is set to -10°C, and the freeze-drying is performed for 10 hours;
[0089] 2. Preparation of modified granules containing peppermint extract
[0090] Put the SiO2 porous gel powde...
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