Nano cellulose glass fiber composite filter material as well as preparation method and application thereof
A technology of nano-cellulose and glass fiber, which is applied in the direction of synthetic cellulose/non-cellulose material pulp/paper, fiber raw material treatment, filtration and separation, etc. Flocculation and other problems, achieve simple manufacturing process, solve the effect of weak bonding strength and low resistance
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[0044] A preparation method of novel nanocellulose / glass fiber composite filter material, comprising the steps of:
[0045] (1) After immersing the fibrillable plant fiber pulp board in water for a certain period of time, it is dispersed in water by a decomposer to obtain a uniform fiber suspension, which is then filtered, wrung out and balanced for later use.
[0046] (2) Obtaining nanocellulose by physical or chemical treatment, by washing, quantifying, and ultrasonically obtaining nanocellulose solution;
[0047] (3) Add water and a dispersant to the glass fiber raw material to uniformly disperse the slurry to obtain a slurry, which is sequentially deslagged, diluted, formed, and dehydrated to form a wet paper sheet with uniform thickness.
[0048] (4) The nanocellulose solution is coated on the surface of the glass fiber paper by coating to form a nanocellulose coating.
[0049] (5) Drying and molding.
[0050] In the step (1), the fibrillable plant fiber pulp board is o...
Embodiment 1
[0070] (1) Soak the coniferous wood commercial pulp board in deionized water for 4 hours to obtain a slurry with a pulp concentration of 1%; then put the soaked slurry into a deflagger for 20 minutes, and the speed of the demineralizer is 1000 rpm / min , wring out after dissolving, and equilibrate the moisture at 4°C for 24 hours before use.
[0071] (2) Prepare nanocellulose by chemical method TEMPO oxidation method, then wash, and vibrate by ultrasonic wave under 200KW power, obtain the clear and transparent solution that nanocellulose concentration is 0.1%wt.
[0072] (3) Add water and sulfuric acid after the microfiber glass wool and glass fiber chopped strands are proportioned according to the set ratio, and evenly obtain a slurry with a concentration of 1.5wt% and a pH of 3.2 through a high-frequency disintegrator; After deslagging, it is diluted to a pulp suspension with a concentration of 0.45 wt%, formed by a fourdrinier machine, dehydrated to form a wet paper sheet, a...
Embodiment 2
[0077] (1) Soak the hardwood commercial pulp board in deionized water for 6 hours to obtain a slurry with a pulp concentration of 5%; then put the soaked slurry into a deflagger for 30 minutes, and the speed of the demineralizer is 2000 rpm / min , wring out after dissolving, and equilibrate the moisture at 4°C for 24 hours before use.
[0078] (2) The nanocellulose was prepared by chemical acid hydrolysis, then washed, and oscillated by ultrasound at a power of 1000KW to obtain a clear and transparent solution with a nanocellulose concentration of 1.5%wt.
[0079] (3) Add water and sulfuric acid after the microfiber glass wool and glass fiber chopped strands are proportioned according to the set ratio, and stir to obtain a slurry with a concentration of 1.0wt% and a pH of 3.0 through a high-frequency disintegrator; After deslagging, it is diluted to a pulp suspension with a concentration of 0.35wt%, formed by a fourdrinier machine, dehydrated to form a wet paper sheet, and drie...
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