Ceramic support for microwave magnetron and preparation method of ceramic support
A support and ceramic matrix technology, which is applied in the field of metallized ceramic processing, can solve the problems of easy oxidation of aluminum nitride ceramics, achieve the effect of improving ceramic performance, density and mechanical properties, and reducing raw material costs and energy consumption costs
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Embodiment 1
[0037] Embodiment 1: The ceramic support body for microwave magnetron comprises a ceramic substrate and a metallized layer, wherein the ceramic substrate and its preparation method
[0038] The raw material formula components of the ceramic matrix in the ceramic support body in parts by weight: 75 parts of silicon carbide-triazole silane-aluminum nitride mesh matrix, 20 parts of blast furnace slag, 3 parts of dispersant and 2 parts of defoaming agent. Wherein, the dispersant is sodium hexametaphosphate, and the defoaming agent is alkyl silicone oil.
[0039] According to the preparation method of the ceramic matrix of above-mentioned formula composition, comprise the following steps:
[0040] A1. Preparation of silicon carbide-triazole silane-aluminum nitride mesh film substrate:
[0041] Place the aluminum nitride ceramic powder in a 5% oxygen atmosphere, and oxidize it at 1000° C. for 30 minutes to obtain an aluminum oxide film on the surface of the aluminum nitride ceramic...
Embodiment 2
[0049] Embodiment 2: The ceramic support body for microwave magnetron comprises a ceramic substrate and a metallized layer, wherein the ceramic substrate and its preparation method
[0050] The raw material formula components of the ceramic matrix in the ceramic support body in parts by weight: 77 parts of silicon carbide-triazole silane-aluminum nitride mesh matrix, 15 parts of blast furnace slag, 5 parts of sodium hexametaphosphate and 3 parts of alkyl silicone oil.
[0051] The preparation method of the ceramic matrix in Example 2 is the same as in Example 1, and the specific steps refer to Example 1. It is worth noting that in the A1 step, 1-phenyl-3-hydroxyl-1,2,4-triazole, The mass ratio of sodium ethoxide solution and 3-chloropropyltrimethoxysilane is 1:1:2, the mass ratio of silicon carbide powder and triazole silane compound is 1:2, the surface modified silicon carbide and oxidized nitrogen The mass ratio of aluminum oxide is 1:7.
Embodiment 3
[0052] Embodiment 3: The ceramic support body for microwave magnetron comprises a ceramic substrate and a metallized layer, wherein the ceramic substrate and its preparation method
[0053] The raw material formula components of the ceramic matrix in the ceramic support body in parts by weight: 83 parts of silicon carbide-triazole silane-aluminum nitride mesh matrix, 12 parts of blast furnace slag, 4 parts of sodium hexametaphosphate and 1 part of alkyl silicone oil.
[0054] The preparation method of the ceramic matrix in Example 3 is the same as in Example 1, and the specific steps refer to Example 1. It is worth noting that in the A1 step, 1-phenyl-3-hydroxyl-1,2,4-triazole, The mass ratio of sodium ethoxide solution and 3-chloropropyltrimethoxysilane is 1:2:1, the mass ratio of silicon carbide powder and triazole silane compound is 1:3, the surface modified silicon carbide and oxidized nitrogen The mass ratio of aluminum oxide is 1:8.
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