Natural antioxidant and preparation method thereof
A natural antioxidant and antioxidant technology, which can be used in food ingredients as antioxidants, food ingredients containing natural extracts, and food ingredients as coating agents, etc. Attenuates ultraviolet radiation, blocks oxygen, and scavenges free radicals
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Embodiment 1
[0026] 1. A natural antioxidant, its composition includes by weight: 25 parts of water-soluble active ingredients, 37 parts of oil active ingredients, and 12 parts of surfactants.
[0027] 2. Extract water-soluble active ingredients:
[0028] a. Dry and pulverize the chili seeds, disperse them in distilled water, add a compound enzyme with 7% weight of chili seed powder for enzymolysis, and then recycle the enzyme. After recycling, use 25kV / cm electric field strength, 13μs pulse width, 725Hz Perform PEF treatment at the pulse frequency for 7s, and filter to obtain filter residue and filtrate;
[0029] b. The filtrate in step a was extracted twice using ethyl acetate as a solvent with a solid-to-liquid ratio of 1.5:3, and the extract phases were combined, evaporated under reduced pressure to remove the solvent, spray-dried, and pulverized to obtain a water-soluble active ingredient.
[0030] Further, the compound enzyme is prepared by mixing protease, cellulase and pectinase i...
Embodiment 2
[0040] 1. A natural antioxidant, its composition includes by weight: 20 parts of water-soluble active ingredients, 30 parts of oil active ingredients, and 8 parts of surfactants.
[0041] 2. Extraction of water-soluble active ingredients:
[0042] a. Dry and crush the chili seeds, disperse them in distilled water, add a compound enzyme with 4% weight of chili seed powder for enzymolysis, and then recycle the enzyme. Perform PEF treatment at the pulse frequency for 5s, and filter to obtain filter residue and filtrate;
[0043] b. The filtrate in step a was extracted twice using ethyl acetate as a solvent with a solid-to-liquid ratio of 1:2, the extract phases were combined, the solvent was removed by distillation under reduced pressure, spray-dried, and pulverized to obtain a water-soluble active ingredient.
[0044] Further, the compound enzyme is prepared by mixing protease, cellulase and pectinase in a mass ratio of 4:10:9.
[0045] Further, the recovery treatment is to us...
Embodiment 3
[0054] 1. A natural antioxidant, its composition includes by weight: 30 parts of water-soluble active ingredients, 45 parts of oil active ingredients, and 16 parts of surfactants.
[0055] 2. Extraction of water-soluble active ingredients:
[0056] a. Dry and pulverize the chili seeds, disperse them in distilled water, add a compound enzyme with 9% weight of chili seed powder for enzymolysis, and then recycle the enzyme. After recycling, use 25kV / cm electric field strength, 13μs pulse width, 725Hz The pulse frequency is carried out PEF processing 8s, filter to obtain filter residue and filtrate;
[0057] b. The filtrate in step a was extracted twice using ethyl acetate as a solvent with a solid-to-liquid ratio of 1.5:4, the extract phases were combined, the solvent was removed by distillation under reduced pressure, spray-dried, and pulverized to obtain a water-soluble active ingredient.
[0058] Further, the compound enzyme is prepared by mixing protease, cellulase and pecti...
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