Antibacterial material, antibacterial product and preparation method thereof
A technology of antibacterial materials and antibacterial products, applied in botanical equipment and methods, fungicides, chemicals for biological control, etc., can solve the problems of poor slow release effect, easy discoloration, etc. Impact resistance, strong bactericidal effect
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Embodiment 1
[0054] (1) Preparation of metal support zirconium phosphate intermediate
[0055] Mix the cubic zirconium phosphate prepared above with ethanol to prepare a 10wt% slurry, then mix and stir with ethyl orthosilicate for 5 hours at room temperature to carry out ion exchange, then dry and filter for later use, ethyl orthosilicate accounts for cubic phosphoric acid The mass ratio of zirconium is 2‰.
[0056] (2) The metal carrier zirconium phosphate antibacterial agent that the present embodiment makes is nano silver-loaded zirconium phosphate antibacterial agent, and its preparation process is as follows:
[0057] The metal carrier zirconium phosphate intermediate prepared above was mixed with deionized water to prepare a 10wt% dispersion liquid, and then mixed with a silver nitrate aqueous solution with a mass concentration of 2wt% at a temperature of 80°C for 8 hours for ion exchange, and then obtained The products are dried and sintered in turn to obtain nano silver-loaded zir...
Embodiment 2
[0063] In the preparation of the metal-supported zirconium phosphate intermediate in this example, 15 wt% cubic zirconium phosphate slurry and ethyl orthosilicate were mixed and stirred at room temperature for 6 hours, and then dried and filtered for later use. Ethyl orthosilicate accounted for cubic zirconium phosphate The mass ratio is 2‰.
[0064] In the preparation of the nano-loaded copper zirconium phosphate antibacterial agent, the prepared 10wt% dispersion liquid and the mass concentration of 2wt% copper nitrate aqueous solution were stirred at a temperature of 70°C for 8h to perform ion exchange, and the copper nitrate accounted for the metal carrier zirconium phosphate The mass ratio of the intermediate was 5%.
[0065] In the preparation of the antibacterial material, take the nanometer copper-loaded zirconium phosphate antibacterial agent and the stainless steel powder, the ratio of the nanometer copper-loaded zirconium phosphate antibacterial agent to the mass of ...
Embodiment 3
[0068] In the preparation of the metal-supported zirconium phosphate intermediate in this example, 15 wt% cubic zirconium phosphate slurry and ethyl orthosilicate were mixed and stirred at room temperature for 6 hours, and then dried and filtered for later use. Ethyl orthosilicate accounted for cubic zirconium phosphate The mass ratio is 5‰.
[0069] In the preparation of the nano-zinc-loaded zirconium phosphate antibacterial agent, the concentration of the metal carrier zirconium phosphate intermediate dispersion is 15wt%, and the dispersion and the mass concentration of 2wt% zinc nitrate aqueous solution are mixed and stirred at 60°C for 6h; and the zinc nitrate The ratio to the mass of the metal carrier zirconium phosphate intermediate is 4%.
[0070] In the preparation of the antibacterial material, take the nano-zinc-loaded zirconium phosphate antibacterial agent and the stainless steel powder, the ratio of the nano-zinc-loaded zirconium phosphate antibacterial agent to t...
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