High-temperature-resistant epoxy putty and preparation method thereof
An epoxy putty, high temperature resistant technology, applied in fire-resistant coatings, filling slurry, etc., to improve performance, increase specific surface area, enhance stability and ductility
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Embodiment 1
[0031] 1. A high-temperature-resistant epoxy putty is composed of a main resin and a curing agent; the main resin is composed of 22 parts by weight of heat-resistant coating, 13 parts of silicone resin, 13 parts of epoxy resin, nitrogen 48 parts of nanometer ceramic micropowders, 6 parts of xylenes; Described curing agent is 7 parts of aromatic amine curing agents by weight.
[0032] Further, the composition of the heat-resistant coating is calculated by weight: 12 parts of zirconia, 20 parts of γ-alumina, 6 parts of graphene, and 22 parts of ethylene glycol.
[0033] Further, the preparation method of described heat-resistant paint is:
[0034] a. Add γ-Al 2 o 3 Carry out calcination at a temperature of 480°C for 1.5h, blend and grind with graphene after cooling, add ethylene glycol and stir at a rate of 600rpm for 30min to obtain a mixture;
[0035] b. obtained by mixing and stirring zirconia and the mixture obtained in step a, drying and pulverizing in an oven at 65°C. ...
Embodiment 2
[0047] 1. A high-temperature-resistant epoxy putty is composed of a main resin and a curing agent; the main resin is composed of 20 parts by weight of heat-resistant coating, 10 parts of silicone resin, 10 parts of epoxy resin, nitrogen 45 parts of nano ceramic micropowder, 4 parts of acrylic acid diluent (X-5); Described curing agent is 5 parts of alicyclic amines by weight.
[0048] Further, the composition of the heat-resistant coating is as follows in parts by weight: 10 parts of zirconia, 17 parts of γ-alumina, 4 parts of graphene, and 16 parts of ethylene glycol.
[0049] Further, the preparation method of described heat-resistant paint is:
[0050] a. Calcining γ-alumina at a temperature of 480°C for 1.5h, blending and grinding with graphene after cooling, adding ethylene glycol and stirring at a rate of 500rpm for 40min to obtain a mixture;
[0051] b. obtained by mixing and stirring zirconia and the mixture obtained in step a, drying and pulverizing in an oven at 60°...
Embodiment 3
[0063] 1. A high-temperature-resistant epoxy putty is composed of a main resin and a curing agent; the main resin is composed of 25 parts by weight of heat-resistant coating, 115 parts of silicone resin, 15 parts of epoxy resin, nitrogen 50 parts of nanometer ceramic micropowder, 10 parts of cyclohexanone; Described curing agent is 10 parts of epoxide addition polyamines by weight.
[0064] Further, the composition of the heat-resistant coating is as follows in parts by weight: 15 parts of zirconia, 24 parts of γ-alumina, 8 parts of graphene, and 28 parts of ethylene glycol.
[0065] Further, the preparation method of described heat-resistant paint is:
[0066] a. Calcining γ-alumina at a temperature of 480°C for 1.5h, blending and grinding with graphene after cooling, adding ethylene glycol and stirring at a rate of 700rpm for 20min to obtain a mixture;
[0067] b. obtained by mixing and stirring zirconia and the mixture obtained in step a, drying and pulverizing in an oven ...
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