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Preparation method of flame-retardant adhesive for artificial board

A technology for flame retardant adhesives and sheets, applied in the directions of adhesives, adhesive additives, adhesive types, etc., can solve problems such as adverse effects, loss of flame retardant effect, increase the complexity of flame retardant process, etc., to achieve small particle size, good quality Flame retardant effect, effect of promoting char formation

Inactive Publication Date: 2021-01-01
彭静
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Drying treatment is required after dipping, which increases the complexity of the flame retardant process, and is limited by the permeability of the wood material itself, and has the disadvantages of losing the flame retardant effect due to the precipitation and loss of the flame retardant. Most Outstanding Issues in Technology
The additive method has the problem of the adaptability of the adhesive and the flame retardant. If the adaptability is poor, it will not only be impossible to mix and use, but also have a negative impact on the bonding performance of the adhesive. This process also increases the complexity of production.
The disadvantage of fire retardant coating treatment is that the opacity of most fire retardant coatings cannot meet the decoration requirements in the use of wood materials.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0030]In parts by weight, weigh 40 parts of 15% formaldehyde solution, 20 parts of urea, and 20 parts of melamine. Add 1 / 2 part of urea and 1 / 2 part of melamine to the formaldehyde solution and add dropwise The pH of 1% sodium hydroxide solution was adjusted to 7, under the water bath condition of 80~90℃, stirred at 200r / min for 40min, and kept warm to obtain the reaction solution. The remaining 1 / 2 part by weight of urea and the remaining 1 / 2 parts by weight of melamine was added to the reaction solution, 10% by mass of ammonia was added dropwise to adjust the pH to 8, stirred at a speed of 300r / min for 40 minutes under a water bath at 80°C, and cooled at room temperature to obtain a melamine-modified urea-formaldehyde resin;

[0031]Then, in parts by weight, weigh 20 parts of magnesium sulfate hexahydrate, 8 parts of sodium hydroxide, 4 parts of methyltrimethoxysilane, and 300 parts of deionized water, and add 1 / 3 parts of magnesium sulfate hexahydrate by weight. In deionized water,...

Embodiment 2

[0034]In parts by weight, weigh 50 parts of 15% formaldehyde solution, 25 parts of urea, and 25 parts of melamine respectively, add 1 / 2 part of urea and 1 / 2 part of melamine to the formaldehyde solution, and add dropwise The pH of 1% sodium hydroxide solution was adjusted to 7.5, stirred at 225r / min for 50min under the water bath condition of 85℃, and kept warm to obtain the reaction solution. The remaining 1 / 2 weight part of urea and the remaining 1 / 2 weight Part of melamine was added to the reaction solution, 10% by mass of ammonia was added dropwise to adjust the pH to 8.5, stirred at 325r / min for 50 minutes in a water bath at 85°C, and cooled at room temperature to obtain a melamine-modified urea-formaldehyde resin;

[0035]Then, in parts by weight, weigh 25 parts of magnesium sulfate hexahydrate, 10 parts of sodium hydroxide, 5 parts of methyltrimethoxysilane, and 375 parts of deionized water, and add 1 / 3 parts of magnesium sulfate hexahydrate by weight. In deionized water, stir a...

Embodiment 3

[0038]In parts by weight, weigh 60 parts of 15% formaldehyde solution, 30 parts of urea, and 30 parts of melamine. Add 1 / 2 part of urea and 1 / 2 part of melamine to the formaldehyde solution and add dropwise The pH of 1% sodium hydroxide solution was adjusted to 8, under the condition of 90℃ water bath, stirred at 250r / min for 60min, and kept warm to obtain the reaction solution. The remaining 1 / 2 weight part of urea and the remaining 1 / 2 weight Part of melamine was added to the reaction solution, 10% by mass of ammonia was added dropwise to adjust the pH to 9, and stirred at a speed of 350r / min for 60 minutes in a water bath at 90°C, and cooled at room temperature to obtain a melamine-modified urea-formaldehyde resin;

[0039]Then, in parts by weight, weigh 30 parts of magnesium sulfate hexahydrate, 12 parts of sodium hydroxide, 6 parts of methyltrimethoxysilane, and 450 parts of deionized water, and add 1 / 3 parts of magnesium sulfate hexahydrate by weight. In deionized water, stir at ...

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Abstract

The invention relates to a preparation method of a flame-retardant adhesive for an artificial board, and belongs to the technical field of adhesives. The flame-retardant adhesive for the artificial board is prepared by adding the modified superfine magnesium hydroxide powder, and the superfine magnesium hydroxide flame retardant can release moisture, absorb heat and reduce the actual temperature of flame on the surface of the board when being heated and decomposed, so that the speed of degrading a polymer into low molecules is reduced. The uniformly released water vapor can dilute the concentration of oxygen on the surface of the wood, so that the combustion on the surface of the wood cannot be continued; the ultrafine uniformly-dispersed magnesium hydroxide flame retardant can react withwood at high temperature to decompose non-combustible gas such as carbon dioxide, and the fire extinguishing effect is achieved by isolating air.

Description

Technical field[0001]The invention relates to a method for preparing a flame-retardant adhesive for artificial boards, and belongs to the technical field of adhesives.Background technique[0002]In recent years, wood materials have been widely used in decoration and building materials. However, the natural flammability of wood products used in homes and public places constitutes a fire hazard. With the popularization of wood products in homes and public places, fire safety issues have become more prominent. Therefore, in order to reduce the occurrence of fires, considering the safety of human life and property, it is necessary to research and develop flame-retardant wood materials and use wood materials with flame-retardant functions, and it is also the most concerned issue in the industry.[0003]The main method of the existing wood material flame retardant technology is to impregnate the flame retardant material into the wood, or mechanically mix the flame retardant material with the ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09J161/30C09J11/04C08G12/38
CPCC08G12/38C08K2003/2224C08K2003/323C09J11/04C09J161/30C08K9/06C08K3/22
Inventor 彭静
Owner 彭静
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