Preparation method of flame-retardant adhesive for artificial board
A technology for flame retardant adhesives and sheets, applied in the directions of adhesives, adhesive additives, adhesive types, etc., can solve problems such as adverse effects, loss of flame retardant effect, increase the complexity of flame retardant process, etc., to achieve small particle size, good quality Flame retardant effect, effect of promoting char formation
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Embodiment 1
[0030]In parts by weight, weigh 40 parts of 15% formaldehyde solution, 20 parts of urea, and 20 parts of melamine. Add 1 / 2 part of urea and 1 / 2 part of melamine to the formaldehyde solution and add dropwise The pH of 1% sodium hydroxide solution was adjusted to 7, under the water bath condition of 80~90℃, stirred at 200r / min for 40min, and kept warm to obtain the reaction solution. The remaining 1 / 2 part by weight of urea and the remaining 1 / 2 parts by weight of melamine was added to the reaction solution, 10% by mass of ammonia was added dropwise to adjust the pH to 8, stirred at a speed of 300r / min for 40 minutes under a water bath at 80°C, and cooled at room temperature to obtain a melamine-modified urea-formaldehyde resin;
[0031]Then, in parts by weight, weigh 20 parts of magnesium sulfate hexahydrate, 8 parts of sodium hydroxide, 4 parts of methyltrimethoxysilane, and 300 parts of deionized water, and add 1 / 3 parts of magnesium sulfate hexahydrate by weight. In deionized water,...
Embodiment 2
[0034]In parts by weight, weigh 50 parts of 15% formaldehyde solution, 25 parts of urea, and 25 parts of melamine respectively, add 1 / 2 part of urea and 1 / 2 part of melamine to the formaldehyde solution, and add dropwise The pH of 1% sodium hydroxide solution was adjusted to 7.5, stirred at 225r / min for 50min under the water bath condition of 85℃, and kept warm to obtain the reaction solution. The remaining 1 / 2 weight part of urea and the remaining 1 / 2 weight Part of melamine was added to the reaction solution, 10% by mass of ammonia was added dropwise to adjust the pH to 8.5, stirred at 325r / min for 50 minutes in a water bath at 85°C, and cooled at room temperature to obtain a melamine-modified urea-formaldehyde resin;
[0035]Then, in parts by weight, weigh 25 parts of magnesium sulfate hexahydrate, 10 parts of sodium hydroxide, 5 parts of methyltrimethoxysilane, and 375 parts of deionized water, and add 1 / 3 parts of magnesium sulfate hexahydrate by weight. In deionized water, stir a...
Embodiment 3
[0038]In parts by weight, weigh 60 parts of 15% formaldehyde solution, 30 parts of urea, and 30 parts of melamine. Add 1 / 2 part of urea and 1 / 2 part of melamine to the formaldehyde solution and add dropwise The pH of 1% sodium hydroxide solution was adjusted to 8, under the condition of 90℃ water bath, stirred at 250r / min for 60min, and kept warm to obtain the reaction solution. The remaining 1 / 2 weight part of urea and the remaining 1 / 2 weight Part of melamine was added to the reaction solution, 10% by mass of ammonia was added dropwise to adjust the pH to 9, and stirred at a speed of 350r / min for 60 minutes in a water bath at 90°C, and cooled at room temperature to obtain a melamine-modified urea-formaldehyde resin;
[0039]Then, in parts by weight, weigh 30 parts of magnesium sulfate hexahydrate, 12 parts of sodium hydroxide, 6 parts of methyltrimethoxysilane, and 450 parts of deionized water, and add 1 / 3 parts of magnesium sulfate hexahydrate by weight. In deionized water, stir at ...
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