Method for preparing assembly type inner wall prefabricated thermal insulation board by using urban solid waste
A prefabricated and thermal insulation board technology, which is applied in the field of building materials, can solve the problems of high cost and not too obvious effect, and achieve the effects of reduced preparation cost, high mechanical strength and good heat insulation performance
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Embodiment 1
[0026] (1) Drying, pulverizing and sieving the solid waste to obtain pretreated solid waste particles with an average particle size of 0.1mm and a moisture content of less than 0.1%;
[0027] (2) Dissolve 2ml of tetrabutyl titanate in 15ml of absolute ethanol, add 1ml of deionized water dropwise, then add a mixture of 0.4ml of 1mol / L hydrochloric acid and 20ml of absolute ethanol to adjust the pH of the solution to 2-3, Perform prehydrolysis treatment at 45°C for 50 minutes to obtain a prehydrolyzed sol;
[0028] (3) Dissolve 1g of zirconium acetylacetonate in a mixture of 20ml of absolute ethanol and 10ml of deionized water, then add 0.1ml of formamide, stir at room temperature and 1000rpm for 20min, and finally add 1ml of the pre-hydrolyzed sol prepared above , and add 3ml of 1,2-propylene oxide, cross-linking reaction at 60°C for 20min, and finally use absolute ethanol for solvent exchange for 20h, and the obtained mixture is heated at a temperature of 270°C and a pressure ...
Embodiment 2
[0031] (1) Drying, pulverizing and sieving the solid waste to obtain pretreated solid waste particles with an average particle size of 0.3mm and a moisture content of less than 0.1%;
[0032] (2) Dissolve 3ml of tetrabutyl titanate in 15ml of absolute ethanol, add dropwise 1.5ml of deionized water, then add a mixture of 0.6ml of 1mol / L hydrochloric acid and 20ml of absolute ethanol to adjust the pH of the solution to 2-3 , pre-hydrolyzed at 55°C for 70 minutes to obtain a pre-hydrolyzed sol;
[0033] (3) Dissolve 2g of zirconium acetylacetonate in a mixture of 40ml of absolute ethanol and 10ml of deionized water, then add 0.3ml of formamide, stir at room temperature and 3000rpm for 40min, and finally add 5ml of the pre-hydrolyzed sol prepared above , and add 4ml of 1,2-propylene oxide, cross-linking reaction at 80°C for 80min, and finally use absolute ethanol for solvent exchange for 24h, and the obtained mixture is heated at a temperature of 300°C and a pressure of 10MPa Under...
Embodiment 3
[0036] (1) Drying, pulverizing and sieving the solid waste to obtain pretreated solid waste particles with an average particle size of 0.2mm and a moisture content of less than 0.1%;
[0037] (2) Dissolve 2ml of tetrabutyl titanate in 15ml of absolute ethanol, add 1.5ml of deionized water dropwise, then add 0.5ml of 1mol / L hydrochloric acid and 20ml of absolute ethanol to adjust the pH of the solution to 2-3 , pre-hydrolyzed at 50°C for 60 minutes to obtain a pre-hydrolyzed sol;
[0038] (3) Dissolve 1g of zirconium acetylacetonate in a mixture of 30ml of absolute ethanol and 10ml of deionized water, then add 0.2ml of formamide, stir at room temperature and 1500rpm for 30min, and finally add 2ml of the pre-hydrolyzed sol prepared above , and add 3ml of 1,2-propylene oxide, cross-linking reaction at 70°C for 30min, and finally use absolute ethanol for solvent exchange for 21h, and put the obtained mixture in a room with a temperature of 280°C and a pressure of 9MPa Under the c...
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