An energy-saving synergist for boiler water treatment
An energy-saving synergist and boiler water technology, applied in water/sewage treatment, water/sludge/sewage treatment, flocculation/sedimentation water/sewage treatment, etc., can solve low cleaning efficiency, lower thermal efficiency, deterioration of steam quality, etc. question
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Embodiment 1
[0038] Prepare modifying agent, this modifying agent is made by following steps:
[0039] Step S11: Add phenol and 25% hydrochloric acid solution into the flask, raise the temperature to 35°C, add 4-methylcyclohexanone dropwise into the flask, pass in nitrogen gas, and react at 60°C for 7 hours. After the end, filter with suction, wash the filter cake 5 times with hot water, and recrystallize from absolute ethanol to obtain intermediate 1;
[0040] Step S12: adding intermediate 1 into a flask filled with tetrahydrofuran, introducing chlorine gas, and reacting for 1 h under light conditions to obtain intermediate 2;
[0041] Step S13: Add intermediate 2, potassium hydroxide, and acetone into the flask, stir at 25°C for 20 minutes, add 1,5-dibromopentane, and reflux for 5 hours to obtain intermediate 3;
[0042] Step S14: Add intermediate 3, acetonitrile and potassium carbonate into the flask, stir at 120° C. for 10 min, then drop trimethylamine solution into the flask, and ref...
Embodiment 2
[0046] Prepare modifying agent, this modifying agent is made by following steps:
[0047]Step S11: Add phenol and 25% hydrochloric acid solution into the flask, raise the temperature to 35°C, add 4-methylcyclohexanone dropwise into the flask, pass in nitrogen gas, and react at 60°C for 8 hours. After the end, filter with suction, wash the filter cake 5 times with hot water, and recrystallize from absolute ethanol to obtain intermediate 1;
[0048] Step S12: adding intermediate 1 into a flask filled with tetrahydrofuran, introducing chlorine gas, and reacting for 1.5 h under light conditions to obtain intermediate 2;
[0049] Step S13: Add intermediate 2, potassium hydroxide, and acetone into the flask, stir at 27.5°C for 25 minutes, add 1,5-dibromopentane, and reflux for 6 hours to obtain intermediate 3;
[0050] Step S14: Add intermediate 3, acetonitrile and potassium carbonate into the flask, stir at 120°C for 15 min, then add trimethylamine solution dropwise into the flask...
Embodiment 3
[0054] Prepare modifying agent, this modifying agent is made by following steps:
[0055] Step S11: Add phenol and 25% hydrochloric acid solution into the flask, raise the temperature to 35°C, add 4-methylcyclohexanone dropwise into the flask, pass in nitrogen gas, and react at 60°C for 9h, and react After the end, filter with suction, wash the filter cake 5 times with hot water, and recrystallize from absolute ethanol to obtain intermediate 1;
[0056] Step S12: adding intermediate 1 into a flask filled with tetrahydrofuran, introducing chlorine gas, and reacting for 2 hours under light conditions to obtain intermediate 2;
[0057] Step S13: Add intermediate 2, potassium hydroxide, and acetone into the flask, stir at 30°C for 30 minutes, add 1,5-dibromopentane, and reflux for 7 hours to obtain intermediate 3;
[0058] Step S14: Add intermediate 3, acetonitrile and potassium carbonate into the flask, stir at 120°C for 20 min, then drop trimethylamine solution into the flask, ...
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