Flexible packaging composite film for solar cell backboard film and preparation method
A solar cell, flexible packaging technology, applied in circuits, photovoltaic power generation, electrical components, etc., can solve the problems of acid and alkali resistance, poor water resistance, etc., and achieve the effect of high hinge characteristics, high impact resistance, and excellent moisture resistance.
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Embodiment 1
[0030] A method for preparing a flexible packaging composite film, comprising the steps of:
[0031] (1) Weighing: Weigh according to the following raw material composition in parts by weight: 20 parts of hexamethylene diisocyanate; 16 parts of ethylene glycol; 1 part of graphene oxide, set aside;
[0032] (2) Preparation of polyurethane prepolymer: mix hexamethylene diisocyanate, catalyst dibutyltin dilauric acid and ethylene glycol, react at 75°C for 2 hours, stop heating and cool to room temperature, wash with ethanol and water After obtaining the polyurethane prepolymer;
[0033] (3) Preparation of flexible bottom film: mix the polyurethane prepolymer prepared in step (2) with graphene oxide, then heat and reflux at 80°C for 6h, stop heating, cast to form a film, and obtain a flexible bottom film after drying ;
[0034] (4) Preparation of flexible packaging composite film: use atomic layer deposition equipment to deposit an inorganic interlayer film on the surface of the...
Embodiment 2
[0036] A method for preparing a flexible packaging composite film, comprising the steps of:
[0037] (1) Weighing: Weigh according to the following raw material compositions in parts by weight: 25 parts of tetramethylene diisocyanate; 14 parts of pentylene glycol; 2 parts of graphene oxide, set aside;
[0038] (2) Preparation of polyurethane prepolymer: After mixing tetramethylene diisocyanate, catalyst dibutyltin dilauric acid and pentylene glycol, react at 85°C for 1.5h, stop heating and cool to room temperature, wash with ethanol, Obtain polyurethane prepolymer after washing with water;
[0039] (3) Preparation of flexible base film: mix the polyurethane prepolymer prepared in step (2) with graphene oxide, then heat and reflux at 100°C for 4.5 hours, stop heating, cast a film, and obtain a flexible base after drying membrane;
[0040] (4) Preparation of flexible packaging composite film: use atomic layer deposition equipment to deposit an inorganic interlayer film on the ...
Embodiment 3
[0042] A method for preparing a flexible packaging composite film, comprising the steps of:
[0043] (1) Weighing: Weighing according to the raw material composition of following parts by weight: 30 parts of isophorone diisocyanate; 12 parts of glycerol; 3 parts of graphene oxide, set aside;
[0044] (2) Preparation of polyurethane prepolymer: After mixing isophorone diisocyanate, catalyst dibutyltin dilauric acid and glycerin, react at 90°C for 1 hour, stop heating and cool to room temperature, After washing with ethanol and washing with water, a polyurethane prepolymer is obtained;
[0045] (3) Preparation of flexible bottom film: mix the polyurethane prepolymer prepared in step (2) with graphene oxide, then heat and reflux at 120°C for 3 hours, stop heating, cast to form a film, and obtain a flexible bottom film after drying ;
[0046](4) Preparation of flexible packaging composite film: use atomic layer deposition equipment to deposit an inorganic interlayer film on the ...
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