Breathable and stretchable nanofiber composite thin film material for friction nano generator and preparation method of breathable and stretchable nanofiber composite thin film material
A technology of nanofibers and composite films, applied in textiles, papermaking, non-woven fabrics, etc., can solve the problems of restricting the development and application of high-performance devices, low output voltage of triboelectric nanogenerators, and poor air permeability, etc., and achieve good triboelectricity Electric effect, guaranteed stretch-recovery performance, thickness controllable effect
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Embodiment 1
[0036] Nano fiber composite films, the following steps:
[0037] 1) Weigh 1.5g PVDF-HFP polymer particles, a glass vial was added 20ml; 10ml of acetone was added - dimethylformamide, a mixed solution, wherein the volume ratio of acetone and dimethyl formamide is 6: 4, using a magnetic stirred for 4h to give the sub-stirred solution electrospinning A;
[0038] 2) Weigh 1.2g SEBS elastomer particles, added to a glass vial 20ml; 10ml toluene was added - dimethylformamide mixed solution, wherein the volume ratio of toluene and dimethylformamide for 85:15, using a magnetic stirrer electrospinning solution obtained was stirred for 4h B;
[0039] 3) The solution A and solution B respectively, into two syringes, connected to an electrostatic spinning machine, adjusting electrospinning parameters (voltage -2kV, 20kV) to carry out electrostatic spinning conjugate, wherein the solution A is introduced rate 0.7ml / h, the solution B was introduced rate 2ml / h, to obtain the nanofiber composi...
Embodiment 2
[0041] Nano fiber composite films, the following steps:
[0042] 1) Weigh 1.5g PVDF-HFP polymer particles, a glass vial was added 20ml; 10ml of acetone was added - dimethylformamide, a mixed solution, wherein the volume ratio of acetone and dimethyl formamide is 6: 4, using a magnetic stirred for 4h to give the sub-stirred solution electrospinning A;
[0043] 2) Weigh 1.2g SEBS elastomer particles, added to a glass vial 20ml; 10ml toluene was added - dimethylformamide mixed solution, wherein the volume ratio of toluene and dimethylformamide for 85:15, using a magnetic stirrer electrospinning solution obtained was stirred for 4h B;
[0044] 3) The solution A and solution B respectively, into two syringes, connected to an electrostatic spinning machine, adjusting electrospinning parameters (voltage -2kV, 20kV) to carry out electrostatic spinning conjugate, wherein the solution A is introduced rate 1.1ml / h, the solution B was introduced rate 2ml / h, to obtain the nanofiber composi...
Embodiment 3
[0046] Nano fiber composite films, the following steps:
[0047] 1) Weigh 1.5g PVDF-HFP polymer particles, a glass vial was added 20ml; 10ml of acetone was added - dimethylformamide, a mixed solution, wherein the volume ratio of acetone and dimethyl formamide is 6: 4, using a magnetic stirred for 4h to give the sub-stirred solution electrospinning A;
[0048] 2) Weigh 1.2g SEBS elastomer particles, added to a glass vial 20ml; 10ml toluene was added - dimethylformamide mixed solution, wherein the volume ratio of toluene and dimethylformamide for 15:85, using a magnetic stirrer electrospinning solution obtained was stirred for 4h B;
[0049] 3) The solution A and solution B respectively, into two syringes, connected to an electrostatic spinning machine, adjusting electrospinning parameters (voltage -2kV, 20kV) to carry out electrostatic spinning conjugate, wherein the solution A is introduced rate 1.6ml / h, the solution B was introduced rate 2ml / h, to obtain the nanofiber composi...
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