Thermal barrier coating with composite vertical crack and quasi-columnar gradient structure and preparation method of thermal barrier coating
A gradient structure, thermal barrier coating technology, applied in the coating, metal material coating process, fusion spraying, etc., can solve the problem of poor thermal shock resistance, poor heat insulation performance, poor internal and interface bonding strength of the coating and other problems to achieve the effect of controllable vertical crack spacing
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[0032] Aiming at the technical problems of this application, this application proposes a method for preparing a thermal barrier coating with composite vertical cracks and quasi-columnar gradient structure, which is carried out in a low-pressure chamber of a plasma spraying system under low vacuum conditions. In the present application, the plasma spraying system under low vacuum conditions may include, in addition to the low-pressure chamber, a substrate clamping control unit, a plasma generation unit located directly above the substrate, and a jet stabilization control unit connected to the plasma generation unit and Powder feeding control unit, in which:
[0033] The substrate clamping control unit is used for clamping the substrate, and controlling the substrate to keep perpendicular to the plasma jet, as well as controlling the temperature of the substrate during spraying and pre-sintering. In this application, the substrate is a carrier that needs to deposit a ceramic coa...
example 1
[0054] The substrate is made of austenitic chromium-nickel stainless steel (commonly known as heat-resistant stainless steel 310S). Austenitic chromium-nickel stainless steel has good oxidation resistance and corrosion resistance. With a high percentage of chromium and nickel, it has good creep strength, can work continuously at high temperatures, and has good high temperature resistance.
[0055] The preparation method is as follows:
[0056] 1) Prepare a rectangular or circular substrate material, and fix the substrate and the substrate clamping control unit through a fixed clamping device;
[0057] 2) Sandblasting the surface of the substrate, and then spraying the bonding layer NiCrAlY with a supersonic flame, with a spray thickness of 100-150 μm;
[0058] 3) Turn on the plasma generating unit, adjust the working gas to be a mixture of argon and helium, the working current is 2000A, turn on the jet stability control unit, and spray a plasma jet with a length of 1500mm to ...
example 2
[0064] The substrate is nickel-based superalloy K465. Nickel-based superalloy K465 has high creep resistance, fatigue resistance and high temperature bearing capacity, and is usually used as the stator blade of the propeller.
[0065] The preparation method is as follows:
[0066] 1) Prepare the substrate, and fix the substrate and the substrate clamping control unit through the fixed clamping device;
[0067] 2) Sandblasting the surface of the substrate, and then spraying the bonding layer NiCrAlY with a supersonic flame, with a spray thickness of 100-150 μm;
[0068] 3) Turn on the plasma generating unit, adjust the working gas to be a mixture of argon and helium, the working current is 2000A, turn on the jet stability control unit, and spray a plasma jet with a length of 1500mm to the substrate;
[0069] 4) Prepare 7YSZ powder with a particle size of 1-30 μm, and feed the powder at a rate of 3-4 g / min. In the low-pressure cabin, feed the 7YSZ powder into the plasma jet at...
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