Novel polyurethane coating for waterproof roll as well as preparation method and application of novel polyurethane coating
A technology of polyurethane coatings and waterproof membranes, applied in the direction of polyurea/polyurethane coatings, coatings, etc., can solve the problems of limited viscosity of bonding materials, poor film-forming quality of coatings, and high surface energy, and achieve strong extensibility and strength. Adhesive long-lasting and efficient effect
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preparation Embodiment 1
[0076] The preparation process of the A component: vacuum dehydrate 418kg polyether 330N under the condition of vacuum degree of 0.01Mpa and temperature of 75°C for 2 hours, then dehydrate the polyether under the condition of temperature of 65°C and nitrogen atmosphere 330N was reacted with 66kg of MDI until the content of untested NCO was 2.3%, then the temperature of the reaction system was lowered to 50°C and discharged under a nitrogen atmosphere to obtain the polyurethane prepolymer, namely component A;
[0077] The preparation process of the B component: heat 100kg of aromatic liquid petroleum resin 35# (purchased from Wuxi Haoxiang Chemical Materials Co., Ltd.) to 75°C, then add 150kg of polyether 330N and stir evenly, then add 200kg of filler talc Powder, after stirring evenly, vacuum dehydrate for 2 hours under the conditions of temperature 105°C and vacuum degree 0.09Mpa, then control the system temperature to 75°C, then add 1kg curing agent MOCA and 0.2kgXY-401, stir...
preparation Embodiment 2
[0080] The preparation process of the A component: 418kg of polyether 220 was vacuum dehydrated for 1.5 hours under the conditions of a vacuum of 0.03Mpa and a temperature of 80°C, and then the polyether was dehydrated at a temperature of 75°C and a nitrogen atmosphere. 220 was reacted with 66kg of MDI until the NCO content was 0.96%, and then the temperature of the reaction system was lowered to 60°C and discharged under a nitrogen atmosphere to obtain the polyurethane prepolymer, which is component A;
[0081] The preparation process of the B component: heat 120kg of aromatic liquid petroleum resin 35# (purchased from Wuxi Haoxiang Chemical Materials Co., Ltd.) to 90°C, then add 150kg of polyether 330N and stir evenly, then add 200kg of filler talc powder, after stirring evenly, vacuum dehydrate for 2 hours at a temperature of 100°C and a vacuum degree of 0.08Mpa, then control the temperature of the system to 70°C, then add 1kg of curing agent MOCA and 0.3kg of XY-401, stir t...
preparation Embodiment 3
[0084] The preparation process of the A component: 278.7kg of polyether 330N and 139.3kg of polyether 220 were mixed uniformly and vacuum dehydrated for 2 hours at a vacuum degree of 0.05Mpa and a temperature of 85°C, and then vacuum dehydrated at a temperature of Polyether 330N and polyether 220 were reacted with 66kg of MDI at 85°C and a nitrogen atmosphere until the unmeasured NCO content was 1.9%, then the temperature of the reaction system was lowered to 50°C and discharged under a nitrogen atmosphere to obtain the obtained The polyurethane prepolymer is the A component;
[0085] The preparation process of the B component: heat 80kg of softened oil AM-18 (purchased from Guangzhou Dagang Petroleum Technology Co., Ltd.) to 140°C, and then add 100kg of C9 petroleum resin T-WP8110 (purchased from Sanjiangyuan Chemical (Henan) Co., Ltd.), stirring continuously until the petroleum resin is completely dissolved in the softened oil, then adjust the system temperature to 110°C and...
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