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Flavored syrup and preparation method thereof

A technology of syrup and flavor, applied in hydrazone preparation, confectionery, confectionary industry, etc., can solve the problems of easy crystallization and precipitation of preservatives, toxic and side effects, and difficulty in redissolving, and achieve safe and non-toxic antibacterial activity, exert antiseptic effect, The effect of high antibacterial activity

Pending Publication Date: 2022-03-22
昆山真金食品有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, when the ethanol solution of the preservative is mixed with the syrup, due to the difference in polarity between the two, turbidity occurs in the part that contacts the syrup, and the preservative is easy to crystallize and precipitate, causing difficulty in redissolving, affecting the antiseptic effect of the syrup, and the ethanol that dissolves the preservative. Bringing it into the syrup affects the color, fragrance and flavor of the syrup. Although potassium sorbate has high water solubility, it is a chemical preservative and has certain toxic and side effects on the human body. Flavored syrup with active high preservatives is a technical problem to be solved at present

Method used

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  • Flavored syrup and preparation method thereof
  • Flavored syrup and preparation method thereof
  • Flavored syrup and preparation method thereof

Examples

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Effect test

Embodiment 1

[0040] The present embodiment provides a chitosan oligosaccharide-based preservative, which is made by the following steps:

[0041] Step A1. Put 0.05 mol of phloretin derivatives in a three-necked flask, add 20 mL of thionyl chloride and 120 mL of DMF, and heat up to reflux for 3 hours. After the reaction, remove DMF and excess thionyl chloride by rotary evaporation to obtain acid chloride Derivatives of corticosteroids;

[0042] Step A2, put 10g of chitosan oligosaccharide in 120mL of acetic acid solution with a mass fraction of 1%, then add 100mL of methanol and stir evenly, transfer it to a three-necked flask, raise the temperature to 60°C, add 120mL of benzaldehyde methanol solution dropwise, and keep the temperature for 2h After the reaction, cool to room temperature, add 5% sodium hydroxide solution to adjust the pH value to 7.0, continue to stir until no flocculent precipitates are produced, filter with suction, collect the precipitate, and remove the precipitate with ...

Embodiment 2

[0051] The present embodiment provides a chitosan oligosaccharide-based preservative, which is made by the following steps:

[0052] Step A1. Put 0.05 mol of phloretin derivatives in a three-necked flask, add 22 mL of thionyl chloride and 140 mL of DMF, and heat up to reflux for 3 hours. After the reaction, remove DMF and excess thionyl chloride by rotary evaporation to obtain acid chloride Derivatives of corticosteroids;

[0053] Step A2, put 11g of chitosan oligosaccharide in 120mL of acetic acid solution with a mass fraction of 1%, then add 100mL of methanol and stir evenly, then transfer to a three-necked flask, raise the temperature to 60°C, add 120mL of benzaldehyde methanol solution dropwise, and keep the temperature for 2h After the reaction, cool to room temperature, add 5% sodium hydroxide solution to adjust the pH value to 7.0, continue to stir until no flocculent precipitates are produced, filter with suction, collect the precipitate, and remove the precipitate wit...

Embodiment 3

[0062] The present embodiment provides a chitosan oligosaccharide-based preservative, which is made by the following steps:

[0063] Step A1. Put 0.05mol of phloretin derivatives in a three-necked flask, add 25mL of thionyl chloride and 150mL of DMF, heat up to reflux for 3 hours, and after the reaction, remove DMF and excess thionyl chloride by rotary evaporation to obtain acid chloride Derivatives of corticosteroids;

[0064] Step A2, put 12g of chitosan oligosaccharide in 120mL of acetic acid solution with a mass fraction of 1%, then add 100mL of methanol and stir evenly, then transfer to a three-necked flask, raise the temperature to 60°C, add 120mL of benzaldehyde methanol solution dropwise, and keep the temperature for 2h After the reaction, cool to room temperature, add 5% sodium hydroxide solution to adjust the pH value to 7.0, continue to stir until no flocculent precipitates are produced, filter with suction, collect the precipitate, and remove the precipitate with a...

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Abstract

The invention relates to flavored syrup and a preparation method thereof, and belongs to the technical field of syrup production. Comprising the following raw materials in percentage by mass: 40%-50% of white granulated sugar, 5%-10% of high fructose corn syrup, 10%-20% of brown granulated sugar, 3%-5% of a mint extract, 0.1%-1% of lemon concentrated juice, 0.01%-0.1% of citric acid, 0.01%-0.1% of malic acid, 0.01%-0.1% of xanthan gum, 0.01%-0.1% of sodium carboxymethyl cellulose, 0.1%-2% of edible essence, 0.01%-0.1% of a pigment, 0.04%-0.1% of a chitosan oligosaccharide-based preservative and the balance of purified water. The preparation method comprises the following steps: heating water to 85 DEG C, adding white granulated sugar, stirring, transferring into a heat preservation tank, adding high fructose corn syrup and brown granulated sugar, carrying out heat preservation stirring, adding residual raw materials, mixing for 1-2 hours, sterilizing and filtering to obtain the flavored syrup, and adding the chitosan oligosaccharide-based preservative and the mint extract to endow the syrup with better flavor and storage performance.

Description

technical field [0001] The invention belongs to the technical field of syrup production, and in particular relates to a flavored syrup and a preparation method thereof. Background technique [0002] Flavored syrup is a compound syrup with various specific flavors formed by adding auxiliary materials such as flavor, color, and acidity adjustment substances based on white sugar. As the main raw material, it is widely used in coffee, wine preparation, and milk tea. It has a very broad application prospect in beverage making. [0003] Syrup contains nutrients such as sugar and protein, and is easily contaminated by mold, yeast or other microorganisms during the preparation process, resulting in the syrup hygiene index standard failing to meet the requirements. In order to prevent the occurrence of mildew, artificial preservatives are usually added during production to curb and delay the proliferation of microorganisms, so that the quality of syrup meets food safety requirements...

Claims

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Application Information

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IPC IPC(8): A23G3/48A23G3/36A23G3/42A23L3/3562C07C249/16C07C251/86
CPCA23G3/48A23G3/364A23G3/42A23L3/3562C07C249/16A23V2002/00C07C251/86A23V2200/10A23V2250/628A23V2250/606A23V2250/61A23V2250/21A23V2250/032A23V2250/044A23V2250/5086A23V2250/51088A23V2250/511Y02A40/90
Inventor 福岛幸治艾卿李娜祖曦曦李昇沈丽李鹏飞
Owner 昆山真金食品有限公司
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