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Preparation method of antibacterial and deodorant regenerated cellulose fiber

A technology of regenerated cellulose and cellulose, applied in the field of fiber, can solve the problem of no antibacterial and deodorization

Active Publication Date: 2022-04-22
南通荣荟新材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] In order to solve the above technical problems, the present invention provides a preparation method of antibacterial and deodorizing regenerated cellulose fibers, by extracting polyphenols from plants, modifying the cellulose to obtain fibers with antibacterial and deodorizing functions, and solving the problem of Solved the problem that ordinary regenerated cellulose fibers have no antibacterial and deodorizing effects

Method used

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  • Preparation method of antibacterial and deodorant regenerated cellulose fiber

Examples

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Effect test

Embodiment 1

[0026] (1) Grind mugwort, extract it ultrasonically at 60°C, the power of ultrasonic extraction is 720W, the frequency is 40KHz, after extraction for 1 hour, perform purification, after purification, dry to obtain plant functional components;

[0027] (2) Stir and mix bamboo cellulose, sodium periodate, and sodium acetate buffer solution with a mass ratio of 5:8:25, and react at 20°C for 4 hours to obtain a dialdehyde cellulose suspension;

[0028] (3) Mix the plant functional components with a mass ratio of 5:80 and the dialdehyde cellulose suspension, and react at 40°C for 2 hours. After the reaction, a polyphenol-cellulose composite material is obtained;

[0029] (4) Mix the polyphenol-cellulose composite material with a mass ratio of 3:97 and a mixed solvent to obtain a functional cellulose solution, and add a thickener bentonite and a coagulation bath to the functional cellulose solution, in which the polyphenol-cellulose The mass ratio of the composite material, bentonit...

Embodiment 2

[0031] (1) Grind the green tea and extract it ultrasonically at 150°C. The power of the ultrasonic extraction is 720W and the frequency is 40KHz. After extraction for 2 hours, it is purified. After purification, it is dried to obtain plant functional components;

[0032] (2) Stir and mix cotton cellulose, sodium periodate, and sodium acetate buffer solution with a mass ratio of 5:9:30, and undergo a modification reaction at 30°C for 5 hours to obtain a dialdehyde cellulose suspension;

[0033] (3) Mix the plant functional components with a mass ratio of 5:85 and the dialdehyde cellulose suspension, and react at 40°C for 2 hours. After the reaction, a polyphenol-cellulose composite material is obtained;

[0034] (4) Mix the polyphenol-cellulose composite material with a mass ratio of 3:97 and a mixed solvent to obtain a functional cellulose solution, add a thickener lauryl alcohol and a coagulation bath to the functional cellulose solution, in which the polyphenol-cellulose The...

Embodiment 3

[0036] (1) Grind the kiwi fruit, extract it ultrasonically at 250°C, the power of the ultrasonic extraction is 720W, and the frequency is 40KHz. After extraction for 3 hours, it is purified and dried after purification to obtain plant functional components;

[0037] (2) Stir and mix cotton cellulose, sodium periodate, and sodium acetate buffer solution with a mass ratio of 5:10:32, and undergo a modification reaction at 35°C for 6 hours to obtain a dialdehyde cellulose suspension;

[0038] (3) Mix the plant functional components with a mass ratio of 5:90 and the dialdehyde cellulose suspension, and react at 80°C for 8 hours. After the reaction, a polyphenol-cellulose composite material is obtained;

[0039] (4) Mix the polyphenol-cellulose composite material with a mass ratio of 3:97 and a mixed solvent to obtain a functional cellulose solution, and add a thickener polyacrylate and a coagulation bath to the functional cellulose solution, in which the polyphenol- The mass ratio...

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Abstract

The invention relates to the technical field of fibers, and discloses a preparation method of antibacterial and deodorant regenerated cellulose fibers.Artemisia argyi, green tea, kiwi fruits and other plants are selected as raw materials and subjected to ultrasonic extraction, polyphenol substances in the plants are extracted, microbial growth can be effectively inhibited, bacteria can be effectively killed, and the antibacterial effect is achieved; polyphenols contain a large number of phenolic hydroxyl groups and can be subjected to condensation, neutralization and other reactions with amido, ammonia and other groups, free peculiar smells in the environment are effectively removed, the purpose of deodorization is achieved, aldehyde groups on dialdehyde cellulose and plant extracted polyphenols are subjected to reaction and covalent crosslinking, long-term adhesion is achieved, loss is not prone to occurring in the washing process, and the washing effect is good. And the antibacterial deodorant fabric has the characteristics of being green and environment-friendly.

Description

technical field [0001] The invention relates to the field of fiber technology, in particular to a method for preparing antibacterial and deodorizing regenerated cellulose fibers. Background technique [0002] Textile products play an irreplaceable role in people's daily life. With the rapid development of economy and social civilization, regenerated cellulose fiber is a renewable fiber prepared from natural cellulose through a series of chemical and physical changes. The regenerated cellulose fiber made of cellulose has the characteristics of good softness, comfort, good hygroscopicity, good dyeing performance and gloss, good biodegradability, easy spinning and processing, and is produced during the manufacturing process. It has little pollution and is an important raw material in the textile industry. In recent years, various functional products have emerged one after another. High-efficiency products such as antibacterial, deodorant, and anti-mite are favored by more and m...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01F2/24D01F1/10D01D1/02D01D5/06
CPCD01F2/24D01F1/103D01D1/02D01D5/06
Inventor 刘逸新宗伟袁旭
Owner 南通荣荟新材料科技有限公司
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