GaN-based light-emitting diode based on C-doped current expansion layer and preparation method of GaN-based light-emitting diode
A technology of light emitting diode and current expansion layer, applied in the field of microelectronics, can solve the problems of affecting the crystal quality of the light emitting quantum well layer, increase the complexity of the process, etc., and achieve the effects of alleviating the current congestion effect, high availability and simple process
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Embodiment 1
[0054] See figure 1 and Figure 2, figure 1A schematic flowchart of a preparation method of a GaN-based light-emitting diode based on a C-doped current spreading layer provided by an embodiment of the present invention, and FIG. 2 is a GaN-based light-emitting diode based on a C-doped current spreading layer provided by an embodiment of the present invention. Process schematic diagram of the fabrication method of the diode. The invention provides a preparation method of a GaN-based light-emitting diode based on a C-doped current spreading layer, and the preparation method of the GaN-based light-emitting diode comprises:
[0055] Step 1, see Figure 2a , select the sapphire substrate layer.
[0056] Step 1.1, cleaning the sapphire substrate layer.
[0057] Step 1.2, under the temperature condition of 900-1200°C, heat treatment for 5-10min on the sapphire substrate layer.
[0058] Specifically, it is placed in the MOCVD reaction chamber of metal organic chemical vapor deposi...
Embodiment 2
[0089] On the basis of Embodiment 1, the present invention also provides a preparation method of a C-doped blue LED with an emission wavelength of 450 nm, the preparation method comprising:
[0090] Step one, heat treatment.
[0091] After the sapphire substrate layer is cleaned, it is placed in the MOCVD reaction chamber, and the vacuum degree of the reaction chamber is reduced to 2×10 -2 Torr; then pass hydrogen into the reaction chamber, and under the condition that the pressure of the MOCVD reaction chamber reaches 20 Torr, the sapphire substrate layer is heated to a temperature of 900° C. and kept for 10 minutes to complete the heat treatment of the sapphire substrate layer.
[0092] Step 2, high temperature nitriding.
[0093] The heat-treated sapphire substrate layer was placed in a reaction chamber with a temperature of 1000° C., and ammonia gas with a flow rate of 3,500 sccm was introduced for nitridation for 5 minutes to complete the nitridation.
[0094] Step 3, g...
Embodiment 3
[0114] On the basis of the first embodiment, the present invention also provides a preparation method of a C-doped green LED with an emission wavelength of 520 nm, the preparation method comprising:
[0115] Step one, heat treatment.
[0116] After cleaning the sapphire substrate layer, it was placed in the MOCVD reaction chamber, and the vacuum degree of the reaction chamber was reduced to 2×10 -2 Torr; then pass hydrogen into the reaction chamber, and under the condition that the pressure of the MOCVD reaction chamber reaches 400 Torr, the sapphire substrate layer is heated to a temperature of 1000° C. and kept for 7 minutes to complete the heat treatment of the sapphire substrate layer.
[0117] Step 2, high temperature nitriding.
[0118] The heat-treated sapphire substrate layer was placed in a reaction chamber with a temperature of 1050° C., and ammonia gas with a flow rate of 3500 sccm was introduced into the nitridation for 4 minutes to complete the nitridation.
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