Aqueous buffing oil with shell/core structure
A technology of core-shell structure and polishing oil, which is applied in the field of polishing oil, can solve the problem of poor gloss of the compound emulsion, achieve the effects of improving production and construction conditions, strong adhesion, and good aging resistance
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Embodiment 1
[0022] Add 126.1g of water and 11.4g of 28% ammonia water to a 1-liter flask, stir, heat up to 60°C, add 51.6g of acrylic resin in batches, then raise the temperature to 80°C, and keep it warm for 2 hours to obtain acrylic acid with a solid content of 27%. resin solution. Add the mixed solution of 82.5g water and 10g sodium lauryl sulfate in this acrylic resin solution, start nitrogen, after stirring for 10 minutes, add the mixed solution of 0.6g potassium persulfate and 12g water, then slowly add dropwise 50g benzene Ethylene monomer, the controlled drop time is 2 hours, and the white translucent seed emulsion with blue light is obtained. After insulated for 30 minutes, continue to add dropwise the mixed monomer of 74g styrene, 45g butyl acrylate, and 1g acrylic acid in the seed emulsion, and the dropping time is 3 hours. A mixed solution of potassium sulfate and 6g of water. After the dropwise addition, keep warm at 80°C for 1 hour; then raise the temperature to 90°C for a...
Embodiment 2
[0024] Add 126.1g of water and 11.4g of 28% ammonia water into a 1-liter flask, stir, heat up to 60°C, add 34.4g of acrylic resin in batches, then raise the temperature to 80°C, and keep it warm for 2 hours to obtain acrylic acid with a solid content of 27%. resin solution. Add the mixed solution of 82.5g water and 10g sodium lauryl sulfate in this acrylic resin solution, start nitrogen, after stirring for 10 minutes, add the mixed solution of 0.6g potassium persulfate and 12g water, then slowly add dropwise 67.2g Styrene monomer, the control drop time is 2 hours, obtains the white translucent seed emulsion with blue light. After insulated for 30 minutes, continue to add dropwise the mixed monomer of 74g styrene, 45g butyl acrylate, and 1g acrylic acid in the seed emulsion, and the dropping time is 3 hours. A mixed solution of potassium sulfate and 6g of water. After the dropwise addition, keep warm at 80°C for 1 hour; then raise the temperature to 90°C for aging for half an...
Embodiment 3
[0026] Add 126.1g of water and 11.4g of 28% ammonia water to a 1-liter flask, stir, heat up to 60°C, add 51.6g of acrylic resin in batches, then raise the temperature to 80°C, and keep it warm for 2 hours to obtain acrylic acid with a solid content of 27%. resin solution. Add the mixed solution of 82.5g water and 10g sodium lauryl sulfate in this acrylic resin solution, start nitrogen, after stirring for 10 minutes, add the mixed solution of 0.6g potassium persulfate and 12g water, then slowly add dropwise 50g benzene Ethylene monomer, control drop time is 1.5 hours, obtains white translucent seed emulsion. All the other formulas and process conditions are with embodiment 1. The particle size of latex particles obtained by this system is relatively large, and the polymerization stability is also slightly poor.
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