Friction-reducing and abrasive composite materials with reactive nanometer inorganic particles/epoxy and production thereof
A technology of nano-inorganic particles and epoxy resin, applied in the chemical field, can solve the problems of establishing chemical connections and unsatisfactory wear resistance, and achieve the effect of simple preparation method, easy implementation, and improved friction and wear performance
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[0019] Soap-free emulsion method: Weigh the dried coupling agent γ-methacryltrimethoxysilane to treat the nanoparticles in a 250mL three-necked bottle, the weight of γ-methacryltrimethoxysilane is 10% of the nanoparticle %, add 70ml of ammonia water (containing 0.4% isobutanol as a dispersant) with a pH of 7 to 8, and ultrasonically disperse for 60 minutes. Move the reaction bottle to an oil bath, pass in argon gas, stir magnetically at a constant speed at room temperature for 3 hours, raise the temperature to 70°C, and add initiator K after constant temperature 2 S 2 o 8 (K 2 S 2 o 8 The concentration in the reaction system is 0.005mol / L), and after 35 minutes, monomers are added dropwise to carry out graft polymerization. After reacting for 10 h, the reaction product was obtained by filtration. The weight ratio of each substance in the reaction system is: monomer / nano particle / solvent=(2-4) / 10 / 100. The obtained graft-modified nanoparticles and the remaining monomers w...
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