Photosensitive inorganic paste composition, sheet-shaped unbaked body, and method of producing plasma display front plate
A technology of plasma display and paste composition, applied in the manufacture of discharge tube/lamp, photoengraving process of pattern surface, manufacture of ships or lead wires, etc., can solve the problems of uneven surface, uneven pattern thickness, etc. , to achieve the effect of improving the fineness of the pattern, preventing uneven thickness of the pattern, preventing deformation and cracking
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experiment example 1
[0232] (preparation of photosensitive inorganic paste composition)
[0233] 22 parts by weight of hydroxypropyl cellulose as a water-soluble cellulose derivative, 14 parts by weight of styrene / hydroxyethyl methacrylate=55 / 45 (weight %) copolymer (Mw=40000) as a Acrylic resin, 60 parts by weight of 2-methacryloylethoxy-2-hydroxypropyl phthalate (trade name: HO-MPP, manufactured by Kyoeisha Chemical Co., Ltd.) as a photopolymerizable monomer , 0.9 parts by weight of 2,2-dimethoxy-2-phenylacetophenone (trade name: IR-651, Norish I type, manufactured by Chiba-Geigy) and 1.8 parts by weight of 2,4-diethyl Thioxanthone (trade name: DETX-S, dehydrogenation type, manufactured by Nippon Kayaku Co., Ltd.) as a photopolymerization initiator, 3.9 parts by weight of butyl tartrate as a plasticizer, 0.1 parts by weight of an azo dye ( Trade name: DyeSS, manufactured by Daito Chemix Corporation) as a UV absorber, and 100 parts by weight of 3-methoxy-3-methylbutyl ketone as a solvent, the ab...
experiment example 2
[0235] (preparation of non-photosensitive inorganic paste composition)
[0236] 45 parts by weight of isobutyl methacrylate / hydroxyethyl methacrylate=60 / 40 (% by weight) copolymer (Mw=70000) as an acrylic resin with one hydroxyl group, and 5 parts by weight of dibutyl tartrate as an extender A plasticizer, and 50 parts by weight of 3-methoxy-3-methylbutyl ketone as a solvent were stirred at 80° C. for 3 hours with a stirrer equipped with a water bath to prepare an organic component solution. Then, 40 parts by weight of the organic component solution (50% solid content) and 80 parts by weight of glass frit having a softening point of 574° C. were kneaded together to prepare a non-photosensitive inorganic paste composition.
experiment example 3
[0238] (Preparation of Composition to Form Combustible Intermediate Layer)
[0239] 4 parts by weight of polyvinyl alcohol (trade name: PVA-235, manufactured by Kuraray Co., Ltd.), and 53 parts by weight of water and 43 parts by weight of isopropyl alcohol as a solvent, the above-mentioned substances were stirred with a stirrer for 12 hours , to prepare the anti-permeation layer composition.
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