Gas barrier resin composition and gas barrier film
A technology of resin composition and gas barrier, applied in the direction of synthetic resin layered products, thin material processing, adhesive type, etc., can solve the problems of reduced post-processing, damage to appearance, low productivity, etc., and achieve excellent gas barrier properties Effect
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[0053] As the preparation method of the coating solution, for example, the method of directly adding the organic compound (B) to the solution or emulsion of the polymer (A) and then stirring it, or dissolving or dispersing it in water or various organic solvents in advance A method in which the organic compound (B) in the polymer (A) is added to the solution or emulsion of the polymer (A) and then stirred.
[0054] In the gas barrier resin composition of the present invention, heat stabilizers, antioxidants, reinforcing agents, pigments, antiaging agents, weather resistance agents, flame retardants, and plasticizers may be added as long as the properties are not impaired. , release agent, lubricant, etc.
[0055] Examples of the heat stabilizers, antioxidants and antiaging agents include hindered phenols, phosphorus compounds, hindered amines, sulfur compounds, copper compounds, halides of alkali metals, or mixtures thereof.
[0056] In addition, examples of reinforcing agent...
Embodiment 1
[0071] Mix 439.1 parts of 1,4-bis(isocyanatomethyl)cyclohexane, 35.4 parts of dimethylolpropionic acid, 61.5 parts of ethylene glycol, and 140 parts of acetonitrile as a solvent, and make The reaction time is 3 hours. Then, this carboxylic acid group-containing polyurethane prepolymer solution was neutralized at 50° C. using 24.0 parts of triethylamine. 267.9 parts of this polyurethane prepolymer solution was dispersed in 750 parts of water using a high-speed disperser, and 35.7 parts of 2-[(2-aminoethyl)amino]ethanol was added to carry out chain extension reaction. Aqueous dispersion 1 of a polyurethane resin having a solid content of 25% by weight was obtained by distilling off acetonitrile. 0.5 part of urea was added to the aqueous dispersion 1 (10 parts) of this polyurethane resin, and it stirred for 30 minutes, and the coating liquid was obtained. This coating liquid was applied to the treated surface side of a biaxially stretched polyethylene terephthalate film having ...
Embodiment 2
[0073] 429.1 parts of 1,3-xylylene diisocyanate, 35.4 parts of dimethylolpropionic acid, 61.5 parts of ethylene glycol, and 140 parts of acetonitrile as a solvent were mixed and reacted at 70° C. for 3 hours under a nitrogen atmosphere. Then, this carboxylic acid group-containing polyurethane prepolymer solution was neutralized at 50° C. using 24.0 parts of triethylamine. 267.9 parts of this polyurethane prepolymer solution was dispersed in 750 parts of water using a high-speed disperser, and chain extension reaction was performed using 35.7 parts of 2-[(2-aminoethyl)amino]ethanol. Acetonitrile was distilled off to obtain a polyurethane resin aqueous dispersion 2 having a solid content of 25% by weight. 0.5 part of urea was added to the aqueous dispersion 2 (10 parts) of this polyurethane resin, and it stirred for 30 minutes, and obtained the coating liquid. This coating solution was applied to the treated side of a biaxially stretched polyethylene terephthalate film with a t...
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