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Pulping method for plant fibre raw material combined with biology

A plant fiber and raw material technology, which is applied in cellulose raw material pulping, fiber raw material processing, textile and paper making, etc. Hemicellulose polysaccharide resource waste and other problems, to achieve good penetration and diffusion performance, reduce chemical consumption, shorten the effect of cooking time

Inactive Publication Date: 2008-04-09
GUANGXI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although these technical solutions have many positive effects, the biggest problem encountered in directly extracting lignin and cellulose with high-boiling alcohol from plant fiber raw materials is that most of the hemicellulose sugars in the raw materials are degraded and dissolved in the cooking raffinate , making it difficult to separate products such as lignin, alcohol, and dissolved sugars
[0008] (1) In the traditional chemical pulping and high-yield pulping process of plant fiber raw materials, there is no pretreatment process for extracting sugars such as hemicellulose from raw materials. This part of sugars is dissolved in waste liquid The lignin in it is basically burned together, and its utilization value is low, resulting in a great waste of resources and environmental pollution;
[0009] (2) The existing organic solvent pulping process does not have a pretreatment process for extracting sugars such as hemicellulose
This part of sugars and lignin are dissolved in the organic solvent residue after cooking. In addition to causing waste of hemicellulose polysaccharide resources and failing to realize the full separation and comprehensive utilization of biomass components, it also increases the amount of sugar and organic solvents. The separation difficulty seriously affects the recycling of organic solvents and the industrialization of organic solvent pulping

Method used

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  • Pulping method for plant fibre raw material combined with biology

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] Embodiment 1: investigate the extraction effect of different holding temperatures and holding times

[0029] (1) Implementation conditions:

[0030] Raw material: dry bagasse 80g, extraction water 480ml;

[0031] Extraction temperature: 80°C, 150°C, 170°C respectively;

[0032]Holding time: 15min, 45min, 90min, 120min, 180min respectively;

[0033] Extract pH value: 6;

[0034] Extraction times: 1 time;

[0035] Liquid ratio: 1:6.

[0036] Other conditions: Combining the above different temperatures and times, 9 experiments were designed. After the extraction, separate and collect the extract, wash the bagasse residue three times with hot water at 50°C to 60°C, collect the washing filtrate, and analyze the total sugars, hexoses, and pentoses.

[0037] (2) Implementation effect

[0038] Extraction temperature

Embodiment 2

[0039] Embodiment 2: investigate the extraction effect of different pH values ​​of the extract

[0040] (1). Implementation conditions:

[0041] Extraction temperature: 150°C;

[0042] The pH values ​​of the extracts are: 6, 8, 10;

[0043] The holding time is respectively: 45min and 90min;

[0044] Raw material and other conditions are with embodiment 1.

[0045] (2).Implementation effect

[0046] Extraction temperature

Embodiment 3

[0047] Embodiment 3: investigate the extraction effect under different liquid ratio conditions.

[0048] The liquid ratio of extraction is respectively: 1: 4, 1: 8, 1: 10; Raw material and other conditions are the same as embodiment 1.

[0049] The implementation effect is as follows:

[0050] Extraction temperature

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Abstract

A method of making refined plant fiber raw material pulping combined with biomass is to extract sugar material such as hemicelluloses by water extractives before digesting pulping by plant fiber raw material or processing wastes of plant fiber raw material. When the products of extraction are separated, the liquid part are used for producing fuel ethanol and / or other products by adopting a biotransformation process or a chemical transformation process; the extraction residue can be made into paper pulp by conventional method or used for extracting lignin or processed into fertilizer. By adopting method of the invention, the extracted sugar material such as hemicelluloses can be recycled. When the solid residue left after extraction is used for making pulp by a traditional chemical method, the black liquid pollution can be alleviated and the treatment load of alkali recovery can be reduced; when the solid residue is used for making pulp by organic solvent method, the proportion of sugar material such as hemicelluloses degraded in the cooking residual liquid can be greatly reduced and the difficulty of separation of sugar material and organic solvent in the cooking residual liquid can be reduced, at the same time, by products---lignin can be obtained.

Description

technical field [0001] The invention belongs to the technical field of the pulping method of plant fiber raw materials combined with biological refining. Background technique [0002] With the increasingly serious problems of energy, resources and environment, biorefinery has become the strategic research direction of countries all over the world. The National Committee of the United States predicts that by 2020, 50% of organic chemicals and materials will be produced from biomass raw materials, and the period from 2000 to 2020 will be a critical period for all countries in the world to vigorously develop biomass energy. It is estimated that by 2010 my country's biomass energy utilization will account for 1% of the total primary energy consumption, and by 2020 it will reach 4%. However, since countries around the world have gradually adjusted their policies to reduce or prohibit the conversion of food (starch) into fuel ethanol, the technology of producing cellulosic ethano...

Claims

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Application Information

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IPC IPC(8): D21C3/22
Inventor 胡湛波王景全柴欣生
Owner GUANGXI UNIV
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