Preparation of super absorbent resin containing potassium and nitrogen
A technology of superabsorbent resin and potassium hydroxide, applied in the direction of organic chemistry, can solve the problems of low gel strength, low water absorption, small variety and quantity, etc., and achieve the effect of good performance and increased income
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Embodiment 1
[0022] Embodiment 1: Weigh 4.7g sodium hydroxide and 0.4g potassium hydroxide, measure 15.0ml deionized water, prepare 25% sodium hydroxide and potassium hydroxide mixed solution (wherein the neutralization degree that potassium hydroxide accounts for 1.7%), neutralize 30.0g (28.6ml) of acrylic acid under the conditions of ice-water bath cooling and stirring. Weigh 5.0g of potato starch, measure 25.0ml of deionized water, mix well under stirring, gelatinize in a water bath at 65°C, then cool to room temperature, add 79.8mg of potassium persulfate initiator and neutralized acrylic acid and acrylic acid solution , under the protection of nitrogen, stirred at room temperature for half an hour to make it evenly mixed. Heat with stirring, control the heating rate, and slowly increase the temperature of the water bath to fully proceed the reaction, and stop stirring when the temperature reaches 80°C. Continue to gradually raise the temperature. When the temperature of the water bat...
Embodiment 2
[0023]Embodiment 2: Weigh 8.0g sodium hydroxide and 0.4g potassium hydroxide, measure 25.0ml deionized water, prepare 25% sodium hydroxide and potassium hydroxide mixed solution (wherein the neutralization degree that potassium hydroxide accounts for 1.7%), neutralize 30.0g (28.6ml) of acrylic acid under the conditions of ice-water bath cooling and stirring. Weigh 5.0g of potato starch, measure 25.0ml of deionized water, mix well under stirring, gelatinize in a 65°C water bath, then cool to room temperature, add 81.2mg of potassium persulfate initiator and neutralized acrylic acid and acrylic acid solution , under the protection of nitrogen, stirred at room temperature for half an hour to make it evenly mixed. Heating under stirring, while controlling the heating rate, slowly increasing the temperature of the water bath, and allowing the reaction to proceed fully, and stopping stirring when the temperature reaches 80°C. Afterwards, gradually increase the temperature. When the...
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