Middle element calcium magnesium and sulfur water-retaining agent and preparation method thereof
A technology of elemental calcium and water-retaining agent, which is applied in the field of agriculture and forestry to achieve the effects of saving water resources, facilitating large-scale production, and saving investment
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Embodiment 1
[0047] Add 0.003 g of N,N'-methylenebisacrylamide and 0.003 g of potassium persulfate to 300 g of acrylic acid solution with a weight concentration of 10% and a neutralization degree of 100% with sodium hydroxide under stirring, and dissolve, Then, 24 grams of mechanically pulverized calcium carbonate and 15 grams of magnesium sulfate (average particle size ≤ 45um) were added, and stirred or ultrasonically dispersed for 10 minutes. After the dispersed mixture was stirred and heated at 40°C for 5 hours in the reactor, the temperature was raised to 30°C and reacted for 5 hours to obtain a polymer product; The method makes it pulverized to 0.1-2.0mm, and finally obtains calcium magnesium sulfur water-retaining agent (granular product).
Embodiment 2
[0049] In 300 grams of acrylic acid solution with a weight concentration of 30% and a degree of neutralization of 80%, add 0.09 grams of N,N'-methylenebisacrylamide and 0.09 grams of potassium persulfate under stirring, dissolve, and then mechanically pulverize them. 72 grams of calcium carbonate and 9 grams of magnesium sulfate (average particle size ≤ 45um) were added, and stirred or ultrasonically dispersed for 10 minutes. After the dispersed mixed material is heated in the reactor at 90°C for 1 hour, the temperature is raised to 10°C and reacted for 1 hour to obtain a polymer product; It is pulverized to 0.1-2.0 mm, and finally calcium magnesium sulfur water-retaining agent (granular product) is obtained.
Embodiment 3
[0051] In 300 g of acrylic acid solution with a weight concentration of 25% and a degree of neutralization of 70%, add 1.5 g of N,N'-methylenebisacrylamide and 0.75 g of potassium persulfate under stirring, dissolve, and then mechanically pulverize it. 37.5 grams of calcium carbonate and 9 grams of magnesium sulfate (average particle size ≤ 45um) were added, and stirred to dissolve. After the mixture is heated at 70°C for 3 hours in the reactor, the temperature is raised to 20°C and reacted for 2 hours to obtain a polymer product; the polymer product is dried at 110°C to a water content of less than 20%, and then pulverized by a mechanical method. 0.1~2.0mm, and finally obtain calcium magnesium sulfur water-retaining agent (granular product).
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