Method for measuring main carbonyl compounds in main stream cigarette smoke
A technology for mainstream smoke and carbonyl compounds of cigarettes, applied in measurement devices, instruments, scientific instruments, etc., can solve problems such as affecting the accuracy of test results, increasing consumption of organic solvents, loss of target compounds, etc. The effect of improving detection efficiency and reducing pollution
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[0032] 1. Reagents and instruments
[0033] Reagents: standard products of formaldehyde, acetaldehyde, acetone, acrolein, propionaldehyde, crotonaldehyde, 2-butanone, and 2,4-dinitrophenylhydrazone derivatives of butyraldehyde, purchased from TCI Company; acetonitrile, purchased from Germany CNW Company; ethyl acetate was purchased from Merck, Germany; absolute ethanol was purchased from ROE Company in the United States; the above reagents were all HPLC pure. All experimental water was deionized water treated by an ultrapure water instrument; 2,4-dinitrophenylhydrazine (DNPH) was an analytically pure reagent; phosphoric acid was an analytically pure reagent; aminomethane was an analytically pure reagent.
[0034] Instruments: SM450 20-channel linear smoking machine; Agilent1200 high performance liquid chromatography; ultraviolet detector (VWD); quaternary solvent manager; Swiss Mettler company AE163 electronic balance with a sensitivity of 0.0001g.
[0035] 2. Utilize the ass...
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