Method for applying polyether-ether-ketone heat-conducting insulating coating
A technology of polyether ether ketone, heat conduction and insulation, applied in the direction of surface coating liquid devices, coatings, special surfaces, etc., can solve the problems of complex construction process, thermal conductivity and insulation can not meet the application needs, etc., to achieve simplification Construction technology, good thermal conductivity, uniform distribution effect
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Embodiment 1
[0038] In a three-necked reaction flask equipped with a thermometer, a nitrogen pipe, a condensing separator, and a stirrer, first add 490 g of refined sulfolane, then add 67.11 g (0.303 mol) of 4,4'-difluorobenzophenone and 33.03 g (0.30mol) hydroquinone (86.4g of polymer can be obtained, solid content is 15%), after adding 74g of xylene, stirring and heating, until it is completely dissolved and when the temperature rises to 80°C, add 34.98 g (10 mol% excess relative to hydroquinone) Na 2 CO 3, and then continue to heat up, when the temperature rises to 150°C, the system starts to azeotrope, xylene and water condense in the water separator, the upper layer of xylene refluxes, the lower layer of water is continuously released, continue to heat up to 190°C with water, and wait for the water to be recovered When the theoretical amount was reached, the upper layer of xylene began to be clear and transparent, and then continued to reflux for 20 minutes, then began to steam out t...
Embodiment 2
[0043] In a three-necked reaction flask equipped with a thermometer, a nitrogen pipe, a condensing separator, and a stirrer, first add 490 g of refined sulfolane, then add 67.11 g (0.303 mol) of 4,4'-difluorobenzophenone and 33.03 g (0.30mol) hydroquinone (86.4g of polymer can be obtained, solid content is 15%), after adding 74g of xylene, stirring and heating, until it is completely dissolved and when the temperature rises to 80°C, add 34.98 g (10 mol% excess relative to hydroquinone) Na 2 CO 3 , and then continue to heat up until the temperature rises to 150°C, the system starts to azeotrope, xylene and water condense in the water separator, the upper layer of xylene refluxes, continue to heat up to 200°C with water, the lower layer of water is continuously released, and the water is recovered When the theoretical amount is reached, the upper layer of xylene begins to be clear and transparent, and then continues to reflux for 20 minutes, then starts to distill the xylene fr...
Embodiment 3
[0045] In a three-necked reaction flask equipped with a thermometer, a nitrogen pipe, a condensing separator, and a stirrer, first add 490 g of refined sulfolane, then add 67.11 g (0.303 mol) of 4,4'-difluorobenzophenone and 33.03 g (0.30mol) hydroquinone (86.4g of polymer can be obtained, solid content is 15%), after adding 74g of xylene, stirring and heating, until it is completely dissolved and when the temperature rises to 80°C, add 34.98 g (10 mol% excess relative to hydroquinone) Na 2 CO 3 , and then continue to heat up until the temperature rises to 150°C, the system starts to azeotrope, xylene and water condense in the water separator, the upper layer of xylene refluxes, continue to heat up to 200°C with water, the lower layer of water is continuously released, and the water is recovered When the theoretical amount is reached, the upper layer of xylene begins to be clear and transparent, and then continues to reflux for 20 minutes, then starts to distill the xylene fr...
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