Method for electrolytically refining crude lead
A technology of electrolytic refining and rough lead, which is applied in the fields of process efficiency improvement, photographic technology, instruments, etc., can solve environmental and human hazards and other problems, and achieve the effects of improving direct recovery rate, overcoming environmental pollution, and improving electrolysis efficiency
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Embodiment 1
[0020] The lead content in crude lead is 98.30%, and the main impurities are 0.0008% tin, 0.8281% antimony, 0.1363% bismuth, 0.5127% arsenic, 0.0795% copper, 0.0006% zinc, 0.1406% silver, and 0.0013% iron. Tartaric acid, sodium hydroxide and lead oxide were all analytically pure.
[0021] Weigh 500 g of crude lead, heat and melt in a muffle furnace at 600 °C for 15 min, take it out, and cast it into an anode plate in a graphite mold with a size of 10 cm × 10 cm.
[0022] Weigh 200 g of lead oxide, 180 g of sodium hydroxide, and 180 g of tartaric acid into 1.5 L of water, stir magnetically at 70°C for 4 h, and filter to obtain an electrolyte solution in which the concentration of lead ions is 110 g / L. Control the electrolysis temperature at 55°C and the current density at 140 A / m 2 , pole distance 4 cm, plate area 9.7 cm×9.9 cm, electrolyte circulation rate 30 mL / min, when the cell voltage rises to 1.0V, take out the anode plate, wash the anode slime and put it into the elec...
Embodiment 2
[0029] The lead content in crude lead is 98.10%, and the main impurities are 0.0008% tin, 0.9106% antimony, 0.1959% bismuth, 0.5451% arsenic, 0.0933% copper, 0.0006% zinc, 0.1521% silver, and 0.0015% iron. Tartaric acid, sodium hydroxide and lead oxide were all analytically pure.
[0030] Weigh 500g of crude lead, heat it in a muffle furnace to 650°C and melt it for 15 minutes, take it out, and cast it into an anode plate in a graphite mold with a size of 10cm×10cm.
[0031] Add 180 g of lead oxide, 210 g of sodium hydroxide, and 210 g of tartaric acid into 1.5 L of distilled water, stir magnetically at 80°C for 4 h, and filter to obtain an electrolyte solution in which the concentration of lead ions is 100 g / L. The electrolysis temperature was controlled at 45°C, the current density was 160 A / m2, the pole distance was 4 cm, the plate area was 9.7 cm×9.9 cm, the electrolyte volume was 1.5 L, and the electrolyte circulation rate was 30 mL / min. When the tank voltage rises to 1....
Embodiment 3
[0038] The lead content in crude lead is 98.30%, and the main impurities are 0.0008% tin, 0.8281% antimony, 0.1363% bismuth, 0.5127% arsenic, 0.0795% copper, 0.0006% zinc, 0.1406% silver, and 0.0013% iron. Tartaric acid, sodium hydroxide and lead oxide were all analytically pure.
[0039] Weigh 500 g of crude lead, heat and melt in a muffle furnace at 600 °C for 15 min, take it out, and cast it into an anode plate in a graphite mold with a size of 10 cm × 10 cm.
[0040] Weigh 100 g of lead oxide, 120 g of sodium hydroxide, and 150 g of tartaric acid into 1.5 L of water, stir magnetically at 70°C for 4 h, and filter to obtain an electrolyte solution in which the concentration of lead ions is 80 g / L. Control electrolysis temperature 40℃, current density 100 A / m 2, pole distance 4 cm, plate area 9.7 cm×9.9 cm, electrolyte circulation rate 8.5 mL / min, when the cell voltage rises to 1.0V, take out the anode plate, wash the anode slime and put it into the electrolyzer to continu...
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