Method for preparation and regulation of surface-roughness ZnO nano-cone or nanorod array
A nanorod array and surface roughening technology, which is applied in the field of nanomaterials, can solve the problems of ZnO nanocone or nanorod surface smoothness and difficult surface roughness control, so as to improve light extraction efficiency, increase specific surface area, and improve photocatalysis. efficiency effect
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[0027] Example 1
[0028] This embodiment is the process of preparing and roughening the ZnO nanocone array.
[0029] (1) Choose glass, plastic, Si wafer, LED or SiO 2 Any one of them is used as the substrate and cleaned;
[0030] (2) Sputter a dense ZnO seed layer with good crystallinity on the substrate at room temperature with a magnetron sputtering apparatus;
[0031] (3) Hydrothermal growth of ZnO nanocone array: Put the substrate with the ZnO seed layer prepared in step (2) into the polytetrafluoroethylene containing the precursor solution of the zinc source (zinc acetate, zinc nitrate or zinc sulfate solution) In the vinyl fluoride reactor, the concentration of the precursor solution of the zinc source is 0.02M-0.1M. The reactor is sealed in a stainless steel kettle jacket. The reactor and the kettle jacket are put together in a thermostat for heating and reaction. The reaction temperature is 80℃-100℃ The reaction time is 2-6 hours. After the reaction, it is cooled to room tem...
Example Embodiment
[0043] Example 2
[0044] This embodiment is the process of preparing and roughening the ZnO nanorod array.
[0045] (1) Choose glass, plastic, Si wafer, LED or SiO 2 Any one of them is used as the substrate and cleaned;
[0046] (2) Sputter a dense ZnO seed layer with good crystallinity on the substrate at room temperature with a magnetron sputtering apparatus;
[0047] (3) Use the hydrothermal method to grow the ZnO nanorod array with the parameters given in the experimental numbers in the following table: Put the substrate with the ZnO seed layer prepared in step (2) into the precursor solution containing the zinc source (zinc acetate , Zinc nitrate or zinc sulfate solution) in the beaker, the concentration of the precursor solution of the zinc source is 0.02M-0.1M, seal it with plastic wrap, and put it in a thermostat for heating reaction. The reaction temperature is 60℃-100℃, and the reaction time is 2- After 6 hours, the reaction was cooled down to room temperature, that is, a ...
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