Method for preparing peanut protein composite fiber by using ionic liquid
A technology of ionic liquid and peanut protein, which is applied in the direction of spinning solution preparation, fiber chemical characteristics, cellulose/protein conjugated artificial filament, etc., can solve the problem of low solubility of peanut protein, high production equipment requirements, high consumption of strong acid and strong Alkali and other problems, to achieve good moisture absorption and air permeability, low cost, uniform reaction effect
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Embodiment 1
[0022] The peanut protein extracted from peanut meal was dissolved in 30% imidazole ionic liquid 1-ethyl-3-methylimidazolium acetate [EMIM]AC to prepare a peanut protein ionic liquid solution with a concentration of 25%. Vinyl alcohol was dissolved in 5% imidazole ionic liquid 1-ethyl-3-methylimidazole acetate [EMIM] AC to obtain a 18% polyvinyl alcohol ionic liquid solution, and the above two The solution is mixed according to the ratio of 1:5, mixed at 65°C for 2-3 hours, then adding boric acid with a solid content of 0.02% and hydrogen peroxide with a solid content of 0.04% (boric acid and hydrogen peroxide are auxiliary agents) to obtain spinning The stock solution, the spinning stock solution is degassed and sprayed by a vertical spinning machine, and then enters the coagulation bath. The coagulation bath includes a mixed solution of sodium sulfate, sulfuric acid and acetic acid with an acidity of 2.6mol / L (acidity is 0.0009-0.0018mol / L). The peanut protein / polyvinyl alco...
Embodiment 2
[0024] Peanut protein extracted from peanut meal was dissolved in 30% imidazole ionic liquids 1-butyl-3-methylimidazole acetate [BMIM]AC and 1-ethyl-3-methylimidazole acetate [EMIM] In the mixed solution of AC (ratio 1:1), a peanut protein ionic liquid solution with a concentration of 20% was prepared, and polyvinyl alcohol was dissolved in an imidazole ionic liquid 1-butyl-3-methylimidazole with a concentration of 20%. Acetate [BMIM]AC and 1-ethyl-3-methylimidazolium acetate [EMIM]AC mixed solution (ratio 1:1), prepared a polyvinyl alcohol ionic liquid solution with a concentration of 18%, the The above two solutions were mixed according to the ratio of 1:4, mixed at 65°C for 3 hours, and sodium tetraborate with a solid content of 0.02% and hydrogen peroxide with a solid content of 0.04% were added to prepare a spinning stock solution, and the spinning stock solution was degassed Afterwards, it is sprayed by a vertical spinning machine and enters a coagulation bath. The coag...
Embodiment 3
[0026] Peanut protein extracted from peanut meal was dissolved in 30% imidazole ionic liquid 1-butyl-3-methylimidazole acetate [BMIM]AC, 1-ethyl-3-methylimidazole acetate [EMIM] ]AC and 1-methyl-3-methylimidazole dimethyl phosphate [MMIM][DMP] (ratio 1:1:1), prepared a peanut protein ionic liquid solution with a concentration of 25% , Dissolve polyvinyl alcohol in 10% imidazole ionic liquid 1-butyl-3-methylimidazole acetate [BMIM]AC, 1-ethyl-3-methylimidazole acetate [EMIM] In the mixed solution of AC and 1-methyl-3-methylimidazolium phosphate [MMIM][DMP] (the ratio is 1:1:1), a polyvinyl alcohol ionic liquid solution with a concentration of 17% was prepared , mix the above two solutions according to the ratio of 1:3, mix at 75°C for 2 hours, add sodium tetraborate with a solid content of 0.02% and hydrogen peroxide with a solid content of 0.04%, to obtain a spinning stock solution, spinning stock solution After defoaming, it is spun by a vertical spinning machine and enters ...
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