Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Liquefied polymer fracturing liquid thickener and preparation method thereof

A fracturing fluid thickener and liquefaction technology, which is applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problems of increasing the consumption of manpower and material resources, affecting the quality of base fluid, and insufficient fracturing fluid volume. Achieve the effect of reducing manpower and material resources input, avoiding waste of liquid preparation, and easy quality control

Active Publication Date: 2013-07-31
北京爱普聚合科技有限公司
View PDF5 Cites 4 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0008] 1) The preparation of base liquid not only requires special equipment for mixing dry powder and water, but also easily produces "fish eyes" of different sizes and local agglomeration, which affects the quality of the base liquid;
[0009] 2) The construction flexibility is small. If there is a special reason that the amount of fracturing fluid is insufficient or the fracturing scale needs to be temporarily increased, it cannot be realized on site;
[0010] 3) There are many types of admixtures required, and the admixture steps are cumbersome, which increases the difficulty of controlling the quality of fracturing fluids;
[0011] 4) The hydration and swelling time of thickener dry powder is long (more than 10 minutes), which increases the consumption of manpower and material resources;
[0012] 5) There is a large amount of base fluid residue (10-30%) in the liquid storage tank after fracturing, which increases the cleaning and treatment cost of the liquid storage tank
[0014] With the current domestic and foreign water-based fracturing fluid demand for guar gum is rapidly increasing, the raw material guar beans cannot expand the planting range due to the limitation of growth conditions, resulting in a shortage of guar gum, and the price is also rising

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Liquefied polymer fracturing liquid thickener and preparation method thereof
  • Liquefied polymer fracturing liquid thickener and preparation method thereof
  • Liquefied polymer fracturing liquid thickener and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0063] Specifically, the preparation method of the liquefied thickener of the present invention comprises the following steps:

[0064] The first step: compounding of water-soluble organic solvents

[0065] Keep the temperature in the kettle at 10-30°C, and sequentially add sulfoxide organic solvents (including but not limited to one or more of dimethyl sulfoxide, dibutyl sulfoxide, n-butyl sulfoxide, etc.) ), amide organic solvents (including but not limited to one or more of dimethylformamide, dimethylacetamide, diethylformamide, etc.), monohydric alcohol organic solvents (including but not limited to ethanol, One or more of n-propanol, isobutanol, etc.) or polyhydric alcohol organic solvents (including but not limited to one or more of ethylene glycol, propylene glycol, glycerol, etc.), formate (including But not limited to one or more of sodium formate, potassium formate, etc.), forming a compound organic solvent system. In the compound system, based on the total mass of...

Embodiment 1

[0076] Preparation and performance test of liquid thickener 1:

[0077] 1) Weigh 78g of dimethyl sulfoxide in the kettle and keep stirring; add 34.6g of dimethylacetamide and stir for 20min; add 15g of n-propanol and 18g of isopropanol and stir for 30min; add 4.5g of sodium formate and stir 10min to obtain the compounded water-soluble organic solvent.

[0078] 2) Keep stirring, add 127.8 g of fracturing fluid thickener powder, and stir for 20 minutes to obtain liquefied thickener 1.

[0079] The product in this embodiment is an emulsion dispersion, and after testing, the density is 1.13g / cm 3 , the gelling time is 15s, and the viscosity of 1.0% liquefied thickener after dissolving is 42mPa.s.

Embodiment 2

[0081] Preparation and performance test of liquid thickener 2:

[0082] 1) Weigh 116g of dibutyl sulfoxide in the kettle and keep stirring; add 24g of dimethylformamide and 26g of diethylformamide and stir for 15min; add 24g of ethanol and stir for 15min; add 10g of potassium formate and stir for 15min , to obtain a compounded water-soluble organic solvent.

[0083] 2) Keep stirring, add 244.4 g of fracturing fluid thickener powder, and stir for 25 minutes to obtain liquefied thickener 2.

[0084] The product in this embodiment is an emulsion dispersion, and after testing, the density is 1.24g / cm 3 , the gelling time is 15s, and the viscosity of 1.0% liquefied thickener after dissolving is 56mPa.s.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
densityaaaaaaaaaa
particle size (mesh)aaaaaaaaaa
densityaaaaaaaaaa
Login to View More

Abstract

The invention discloses a liquefied polymer fracturing liquid thickener, which has the following evaluation indexes: the density is 1.0-1.3g / cm<3>; the gelling time is less than or equal to 15s; and the viscosity of 1.0% the dissolved liquefied polymer fracturing liquid thickener is greater than or equal to 30mPa.s. The invention also discloses a method for preparing the liquefied polymer fracturing liquid thickener.

Description

technical field [0001] The present invention relates to an ultra-fast dissolving liquid polymer fracturing fluid thickener (hereinafter referred to as "liquid thickener") for convenience of description. [0002] The present invention also relates to a method for preparing the above-mentioned liquefied thickener. Background technique [0003] Water-based fracturing fluid is an important technology for enhancing oil and gas recovery. In the water-based fracturing process, fine powdered solid fracturing fluid thickeners are generally used, such as guar gum dry powder, synthetic polymer thickener dry powder, etc. The dispersibility and hydration viscosity of the thickener determine the fracturing construction technology, fracturing quality and fracturing cost. [0004] The current fracturing construction technology is generally as follows: [0005] The first step is to prepare the base liquid, disperse the thickener dry powder in water, and fully swell within a certain period...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
Patent Type & Authority Applications(China)
IPC IPC(8): C09K8/68
CPCC08J3/096C08J2325/18C08J2333/02C09K8/68C09K8/882
Inventor 郑焰李树盛罗于建白小丹乔磊
Owner 北京爱普聚合科技有限公司
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products