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Silicon carbide ceramic rotor material prepared through gel injection molding and preparation method thereof

A technology of gel injection molding and silicon carbide ceramics, which is applied in the field of aluminum alloy melt purification treatment, can solve the problems of difficult silicon carbide ceramic rotors, close-fitting forming, large workload, etc. The effect of high density, meeting the requirements of processing and use

Active Publication Date: 2014-02-05
重庆多耐达汽车零部件有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

At present, although some researches have been carried out on the development of silicon carbide ceramic rotor materials for rotary blowing based on extrusion molding, calendering molding and / or injection molding at home and abroad, they are still limited to laboratories and experimental factories. It has not yet entered the stage of industrial mass production. The main reason is that it is difficult to prepare silicon carbide ceramic rotors by these traditional forming methods, which leads to a large workload and high cost of subsequent mechanical processing.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0015] Initial ceramic slurry formulation: 650 grams of 40um silicon carbide; 320 grams of 40um silicon; 12 grams of alumina; 9 grams of lanthanum oxide and 9 grams of yttrium oxide.

[0016] Add the above materials into the monomer premix solution to obtain the initial ceramic slurry, and at the same time adjust the amount of the monomer premix solution so that the solid phase volume fraction of the initial ceramic slurry is 55Vol%; ball mill the initial ceramic slurry for 4 hours to obtain To stabilize the ceramic slurry, the stabilized ceramic slurry was vacuum defoamed for 20 minutes at room temperature, and then ammonium persulfate accounting for 0.5wt% of the defoaming slurry and 0.2wt% of the defoaming slurry were added to the defoaming ceramic slurry. % of tetramethylethylenediamine, and stir well to make it evenly mixed; inject the defoaming ceramic slurry added with ammonium persulfate and tetramethylethylenediamine into the metal mold, and keep it in the incubator at...

Embodiment 2

[0018] Initial ceramic slurry formulation: 750 grams of 50um silicon carbide; 220 grams of 40um silicon; 12 grams of alumina; 9 grams of lanthanum oxide and 9 grams of yttrium oxide.

[0019] Add the above materials into the monomer premix solution to obtain the initial ceramic slurry, and at the same time adjust the amount of the monomer premix solution so that the solid phase volume fraction of the initial ceramic slurry is 55Vol%; ball mill the initial ceramic slurry for 4 hours to obtain To stabilize the ceramic slurry, the stabilized ceramic slurry was vacuum defoamed for 20 minutes at room temperature, and then ammonium persulfate accounting for 0.5wt% of the defoaming slurry and 0.2wt% of the defoaming slurry were added to the defoaming ceramic slurry. % of tetramethylethylenediamine, and stir well to make it evenly mixed; inject the defoaming ceramic slurry added with ammonium persulfate and tetramethylethylenediamine into the metal mold, and keep it in the incubator at...

Embodiment 3

[0021] Initial ceramic slurry formulation: 50um silicon carbide 700g; 60um silicon 270g; alumina 12g; lanthanum oxide 9g and yttrium oxide 9g.

[0022]Add the above materials into the monomer premix solution to obtain the initial ceramic slurry, and at the same time adjust the amount of the monomer premix solution so that the solid phase volume fraction of the initial ceramic slurry is 55Vol%; ball mill the initial ceramic slurry for 4 hours to obtain To stabilize the ceramic slurry, the stabilized ceramic slurry was vacuum defoamed for 20 minutes at room temperature, and then ammonium persulfate accounting for 0.5wt% of the defoaming slurry and 0.2wt% of the defoaming slurry were added to the defoaming ceramic slurry. % of tetramethylethylenediamine, and stir well to make it evenly mixed; inject the defoaming ceramic slurry added with ammonium persulfate and tetramethylethylenediamine into the metal mold, and keep it warm at 80°C in the incubator 30 minutes, then demoulding t...

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Abstract

The invention provides a silicon carbide ceramic rotor material prepared through gel injection molding and a preparation method thereof. The ceramic rotor material comprises the following components in percentage by weight: 65-75% of silicon carbide powder, 22-32% of silicon powder, 1.2% of aluminum oxide, 0.9% of lanthanum oxide and 0.9% of yttrium oxide. The method comprises five steps of preparing a monomer premixed solution, preparing initial and stable ceramic slurry, defoaming the stable ceramic slurry, preparing a ceramic biscuit and sintering the ceramic biscuit. The silicon carbide ceramic rotor material prepared by adopting the method disclosed by the invention has the advantages of high compactness and high-temperature oxidation resistance, good thermal shock resistance, slag corrosion resistance and wear resistance and the like, can well meet processing and operating requirements for a silicon carbide ceramic rotor for rotary injection of an aluminum alloy melt, and has a broad market prospect.

Description

technical field [0001] The invention relates to a preparation method of a silicon carbide ceramic material, in particular to a preparation process of a silicon carbide ceramic rotor material for the rotary blowing of an aluminum alloy melt by gel injection molding, and belongs to the field of purification treatment of an aluminum alloy melt . Background technique [0002] Due to its significant advantages such as high specific strength and specific stiffness, excellent electrical and thermal conductivity, good corrosion resistance and oxidation resistance, aluminum alloys have been increasingly widely used in various fields such as aerospace, automobiles, ships and electronics. In recent decades, a lot of research and development have been carried out around the alloying of aluminum alloys, melt purification, refinement and modification, heat treatment and / or forming processes at home and abroad, in order to develop new high-performance aluminum alloy materials and / Or pro...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B35/565C04B35/622
Inventor 杨明波梁晓峰朱翊
Owner 重庆多耐达汽车零部件有限公司
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